1: 2-(1-adamantyl)-4-bromo-1-methoxybenzene With magnesium; ethylene dibromide in tetrahydrofuran
RefluxInert atmosphere;
2: boric acid trimethyl ester in tetrahydrofuran
T=-50 - -40°C; 0.5 h; Inert atmosphere;
3: With hydrogenchloride; water in tetrahydrofuran
参考文献
Kalvinsh, Ivars; Chernobrovijs, Aleksandrs; Tribulovich, Vyacheslav; Labeish, Vladimir
Patent: US2010/113816 A1, 2010 ;
Location in patent: Page/Page column 3 ;
