2,3,3-三氯-1,1,1-三氟丙烷合成路线 (共 9 条)
参考文献
Haszeldine
Journal of the Chemical Society, 1951 , p. 2495,2503
反应条件
hydrogenchloride; zinc in water T=55 - 82°C;
参考文献
US2013/150634 A1, ;
Paragraph 0036; 0037; 0038 ;
反应条件
1,3-bis-(trifluoromethyl)-benzene; hydrogen fluoride; antimony(V) pentachloride
T=-78 - 100°C; P=21446.5 Torr; 22 h; Inert atmosphereAutoclave;
参考文献
HONEYWELL INTERNATIONAL INC.; Zhai, Yian; Poss, Andrew Joseph; Singh, Rajiv Ratna
Patent: US2013/150634 A1, 2013 ;
Location in patent: Paragraph 0028; 0029; 0030 ;
反应条件
hydrogen fluoride; antimony(V) pentachloride
T=-78 - 100°C; P=21446.5 Torr; 17 h; Inert atmosphereAutoclave;
参考文献
HONEYWELL INTERNATIONAL INC.; Zhai, Yian; Poss, Andrew Joseph; Singh, Rajiv Ratna
Patent: US2013/150634 A1, 2013 ;
Location in patent: Paragraph 0025; 0026; 0027 ;
参考文献
Haszeldine
Journal of the Chemical Society, 1951 , p. 2495,2503
反应条件
hydrogen; platinum on activated charcoal in ethanol
P=6080 Torr; 5 h; Ambient temperature;
参考文献
Tanuma, T.; Ohnishi, K.; Okamoto, H.; Miyajima, T.; Morikawa, S.
Journal of Fluorine Chemistry, 1992 , vol. 57, p. 259 - 284
反应条件
hydrogen fluoride; TaClxFy
T=65 - 70°C; Product distribution / selectivity;
参考文献
Honeywell International Inc.
Patent: US2006/58560 A1, 2006 ;
Location in patent: Page/Page column 3 ;
反应条件
hydrogen fluoride; TiClxFy
T=30 - 70°C; Product distribution / selectivity;
参考文献
Honeywell International Inc.
Patent: US2006/58560 A1, 2006 ;
Location in patent: Page/Page column 3 ;
反应条件
alcoholic alkali
und Anlagerung von Chlor an das erhaltene 3.3.3-Trifluor-1-chlor-propen-(1);
参考文献
Henne; Whaley
Journal of the American Chemical Society, 1942 , vol. 64, p. 1157