苄基 alpha-D-吡喃葡萄糖苷合成路线 （共 31 条）
反应条件
methanol; sodium methylate T=20°C; 2 h;
参考文献
Deffieux, Denis; Natangelo, Anna; Malik, Gaelle; Pouysegu, Laurent; Charris, Jaime; Quideau, Stephane
Chemical Communications, 2011 , vol. 47, # 5 p. 1628 - 1630
反应条件
toluene-4-sulfonic acid T=80°C; 5 h;
参考文献
Lau, Kam; Thon, Vireak; Yu, Hai; Ding, Li; Chen, Yi; Muthana, Musleh M.; Wong, Denton; Huang, Ronald; Chen, Xi
Chemical Communications, 2010 , vol. 46, # 33 p. 6066 - 6068
反应条件
1: Ag2O; CaSO4 / diethyl ether / 24 h / 20 °C 2: MeONa / methanol / 0.5 h View Scheme
参考文献
Croatica Chemica Acta, , vol. 77, # 3 p. 491 - 500
反应条件
1: 99 percent / HBr; AcOH / CH2Cl2 / 0 - 20 °C 2: 68 percent / Ag2CO3; I2 / CH2Cl2 / 15 h / 20 °C 3: 99 percent / NaOMe; MeOH / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 124, # 33 p. 9756 - 9767
反应条件
1: 79 percent / HgO (yellow), HgBr2, drierite / CH2Cl2 / 16 h / Ambient temperature 2: 89 percent / 0.02 M NaOCH3 / methanol / 12 h / Ambient temperature View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 28, # 1-11 p. 818 - 823
反应条件
β-D-glucosidase in water T=50°C; 96 h;
参考文献
Kawahara, Eiji; Fujii, Mikio; Kato, Keisuke; Ida, Yoshiteru; Akita, Hiroyuki
Chemical and Pharmaceutical Bulletin, 2005 , vol. 53, # 8 p. 1058 - 1061
反应条件
β-D-glycosidase from Thermus thermophilus in N,N-dimethyl-formamide T=30°C; pH=7; 2 h; aq. phosphate bufferEnzymatic reaction;
参考文献
Marton, Zsuzanna; Tran, Vinh; Tellier, Charles; Dion, Michel; Drone, Jullien; Rabiller, Claude
Carbohydrate Research, 2008 , vol. 343, # 17 p. 2939 - 2946
反应条件
OleD A242V/S132F/P67T triple mutant; tris(hydroxymethyl)methylamine hydrochloride; magnesium chloride T=25°C; pH=8.0; 16 h; Enzymatic reaction; stereoselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 47, # 46 p. 8889 - 8892
反应条件
almond β-glucosidase in acetate buffer; acetonitrile T=50°C; pH=4.4; 72 h;
参考文献
Jerkovic, Igor; Mastelic, Josip
Croatica Chemica Acta, 2004 , vol. 77, # 3 p. 529 - 535
反应条件
hydrogenchloride T=100°C; 3 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 59, # 20 p. 6069 - 6074
