2-丁基-1,2-苯并异噻唑啉-3-酮合成路线 （共 11 条）
反应条件
ammonia in toluene T=50°C; 3 h;
参考文献
Shimizu, Masao; Shimazaki, Teruaki; Yoshida, Tetsuya; Ando, Wataru; Konakahara, Takeo
Tetrahedron, 2012 , vol. 68, # 21 p. 3932 - 3936
反应条件
in toluene T=50°C; 3 h;
参考文献
Shimizu, Masao; Shimazaki, Teruaki; Yoshida, Tetsuya; Ando, Wataru; Konakahara, Takeo
Tetrahedron, 2012 , vol. 68, # 21 p. 3932 - 3936
反应条件
triethylamine in dichloromethane T=-15°C;
参考文献
Pietka-Ottlik, Magdalena; Potaczek, Piotr; Piasecki, Egbert; Mlochowski, Jacek
Molecules, 2010 , vol. 15, # 11 p. 8214 - 8228
反应条件
1: With sulfur; [2,2']bipyridinyl; copper(l) iodide; potassium carbonate in 1-methyl-pyrrolidin-2-one T=110°C; 24 h; Inert atmosphere; 2: With pyridine; N-methoxyamine hydrochloride in 1-methyl-pyrrolidin-2-one T=110°C; 3 h; Inert atmosphere;
参考文献
Krasikova; Katkevics
Chemistry of Heterocyclic Compounds, 2013 , vol. 48, # 11 p. 1684 - 1690
Khim. Geterotsikl. Soedin., 2012 , vol. 48, # 11 p. 1800 - 1807
反应条件
pyridine; N-methoxyamine hydrochloride in various solvent(s) 3 h; Heating;
参考文献
Sano, Tomohumi; Takagi, Toshiyuki; Gama, Yasuo; Shibuya, Isao; Shimizu, Masao
Synthesis, 2004 , # 10 p. 1585 - 1588
反应条件
1,4-diaza-bicyclo[2.2.2]octane; copper(l) iodide; 1,10-phenanthroline; tetra-(n-butyl)ammonium iodide in water T=20 - 160°C; 48.5 h; Inert atmosphere;
参考文献
Wang, Fei; Chen, Chao; Deng, Geng; Xi, Chanjuan
Journal of Organic Chemistry, 2012 , vol. 77, # 8 p. 4148 - 4151
反应条件
1: 97 percent / MeONH2*HCl; pyridine / various solvent(s) / 3 h / Heating View Scheme
参考文献
Synthesis, , # 10 p. 1585 - 1588
反应条件
1: thionyl chloride / Reflux 2: chlorine / tetrachloromethane / 20 °C 3: triethylamine / dichloromethane / -15 °C View Scheme
参考文献
Molecules, , vol. 15, # 11 p. 8214 - 8228
反应条件
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C 2: toluene / 3 h / 50 °C View Scheme
参考文献
Tetrahedron, , vol. 68, # 21 p. 3932 - 3936
反应条件
1: dihydrogen peroxide; methyltrioxorhenium (VII) / dichloromethane; water / 0.5 h / 20 °C 2: ammonia / toluene / 3 h / 50 °C View Scheme
参考文献
Tetrahedron, , vol. 68, # 21 p. 3932 - 3936
