1-苯基-4-戊烯-1-炔合成路线 (共 44 条)
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane T=0°C; 16 h;
参考文献
Ren, Xiao-Feng; Konaklieva, Monika I.; Turos, Edward; Krajkowski, Lynn M.; Lake, Charles H.; et al.
Journal of Organic Chemistry, 1995 , vol. 60, # 20 p. 6484 - 6495
反应条件
Ni(1+)*2C2H3O2(1-)*4H2O; silver(I) acetate; 1,4-di(diphenylphosphino)-butane; zinc in dimethyl sulfoxide
T=100°C; 0.5 h; Reagent/catalystSolventTemperatureTime;
参考文献
Choe, Juseok; Yang, Jiyoung; Park, Kyungho; Palani, Thiruvengadam; Lee, Sunwoo
Tetrahedron Letters, 2012 , vol. 53, # 51 p. 6908 - 6912
反应条件
copper(l) iodide; potassium carbonate; sodium iodide in acetone
T=45°C; 4 h; further reagents, further solvent, further temperature;
参考文献
Bumagin, N. A.; Ponomarev, A. B.; Beletskaya, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 7 p. 1445 - 1448
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 7 p. 1565 - 1569
反应条件
Ni(1+)*2C2H3O2(1-)*4H2O; silver(I) acetate; acetic anhydride; 1,4-di(diphenylphosphino)-butane; zinc in dimethyl sulfoxide
T=100°C; 0.5 h; ConcentrationReagent/catalyst;
参考文献
Choe, Juseok; Yang, Jiyoung; Park, Kyungho; Palani, Thiruvengadam; Lee, Sunwoo
Tetrahedron Letters, 2012 , vol. 53, # 51 p. 6908 - 6912
反应条件
copper(l) iodide; potassium carbonate in N,N-dimethyl-formamide
T=20°C; 0.5 h; further reagents, further solvent, further temperature;
参考文献
Bieber, Lothar W.; da Silva, Margarete F.
Tetrahedron Letters, 2007 , vol. 48, # 40 p. 7088 - 7090
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide
T=50°C; 3 h;
参考文献
Tsuda, Tetsuo; Chujo, Yoshiki; Nishi, Sei-ichi; Tawara, Kunio; Saegusa, Takeo
Journal of the American Chemical Society, 1980 , vol. 102, # 20 p. 6381 - 6384
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
T=75°C; 40 h;
参考文献
Rayabarapu, Dinesh Kumar; Tunge, Jon A.
Journal of the American Chemical Society, 2005 , vol. 127, # 39 p. 13510 - 13511
反应条件
copper(l) iodide; caesium carbonate; diethylphosphinoethane in N,N-dimethyl acetamide; toluene
T=20°C; P=760.051 Torr; 24 h;
参考文献
Inamoto, Kiyofumi; Asano, Narumi; Kobayashi, Koji; Yonemoto, Misato; Kondo, Yoshinori
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 8 p. 1514 - 1516
反应条件
tetra-(n-butyl)ammonium iodide; (Ph3P)2Pd(Ph)(I) in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=20°C;
参考文献
Bumagin, N. A.; Kalinovskii, I. O.; Ponomarev, A. B.; Beletskaya, I. P.
Doklady Chemistry, 1982 , vol. 265, p. 262 - 266
Dokl. Akad. Nauk SSSR Ser. Khim., 1982 , vol. 265, # 5 p. 1138 - 1143
反应条件
lt;Nigt;-PPh3 in tetrahydrofuran
T=40 - 60°C;
参考文献
Dzhemilev, U. M.; Ibragimov, A. G.; Saraev, R. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 2 p. 397 - 401
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 2 p. 429 - 433