反应条件
1.1: 1.39 g / m-chloroperoxybenzoic acid / CH2Cl2; CHCl3
2.1: potassium hydride / tetrahydrofuran / 1.25 h / 0 - 20 °C
2.2: 63 percent / Selectfluor / tetrahydrofuran; dimethylformamide / 2.08 h
3.1: 91 percent / tributyltin chloride; 2,2'-azobisisobutyronitrile; polymethylhydrosiloxane / potassium fluoride / toluene; H2O / 3 h / Heating
View Scheme
参考文献
Wnuk, Stanislaw F.; Bergolla, Luis A.; Garcia Jr., Pedro I.
Journal of Organic Chemistry, 2002 , vol. 67, # 9 p. 3065 - 3071