4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
2 h;
参考文献
Bennett, Christopher J.; Caldwell, Stuart T.; McPhail, Donald B.; Morrice, Philip C.; Duthie, Garry G.; Hartley, Richard C.
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 9 p. 2079 - 2098
1: 69 percent / AlCl3 / chlorobenzene / 90 h / 140 °C
2: 54 percent / potassium hydroxide / ethanol / 119 h
3: 76 percent / H2O2; NaOH / methanol; H2O / 24 h / 0 °C
View Scheme
参考文献
Bennett, Christopher J.; Caldwell, Stuart T.; McPhail, Donald B.; Morrice, Philip C.; Duthie, Garry G.; Hartley, Richard C.
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 9 p. 2079 - 2098