3-(4-硝基苯基)-吡啶合成路线 （共 39 条）
反应条件
copper(l) iodide; C37H51ClFeNPPd; cesium fluoride in N,N-dimethyl-formamide
T=20°C; Stille Cross Coupling; 12 h; Inert atmosphere;
参考文献
Ma, Gaizhi; Leng, Yuting; Wu, Yusheng; Wu, Yangjie
Tetrahedron, 2013 , vol. 69, # 2 p. 902 - 909
反应条件
copper(l) iodide; C52H67ClFeNPPd; cesium fluoride in N,N-dimethyl-formamide
T=110°C; Stille Cross Coupling; 12 h; Inert atmosphere;
参考文献
Ma, Gaizhi; Leng, Yuting; Wu, Yusheng; Wu, Yangjie
Tetrahedron, 2013 , vol. 69, # 2 p. 902 - 909
反应条件
potassium carbonate; cyclopallated ferrocenylimine c in water; N,N-dimethyl-formamide
T=110°C; Suzuki cross-coupling reaction; 5 h;
参考文献
Zhang, Jinli; Zhao, Liang; Song, Maoping; Mak, Thomas C.W.; Wu, Yangjie
Journal of Organometallic Chemistry, 2006 , vol. 691, # 6 p. 1301 - 1306
反应条件
Ti2CO3; tetrakis(triphenylphosphine) palladium(0) in benzene
T=80°C; 12 h;
参考文献
Sato, Makoto; Miyaura, Norio; Suzuki, Akira
Chemistry Letters, 1989 , p. 1405 - 1408
反应条件
caesium carbonate; cyclopallated ferrocenylimine c in water; N,N-dimethyl-formamide
T=110°C; Suzuki cross-coupling reaction; 24 h;
参考文献
Zhang, Jinli; Zhao, Liang; Song, Maoping; Mak, Thomas C.W.; Wu, Yangjie
Journal of Organometallic Chemistry, 2006 , vol. 691, # 6 p. 1301 - 1306
反应条件
triethylamine; tris-(o-tolyl)phosphine; palladium diacetate in acetonitrile
T=125°C; Heck reaction; 20 h;
参考文献
Karig, Gunter; Moon, Maria-Teresa; Thasana, Nopporn; Gallagher, Timothy
Organic Letters, 2002 , vol. 4, # 18 p. 3115 - 3118
反应条件
triethylamine; tris-(o-tolyl)phosphine; palladium diacetate in acetonitrile
T=125°C; Heck reaction; 20 h;
参考文献
Karig, Gunter; Moon, Maria-Teresa; Thasana, Nopporn; Gallagher, Timothy
Organic Letters, 2002 , vol. 4, # 18 p. 3115 - 3118
反应条件
potassium phosphate; palladium dichloride; S-2,2',6,6'-tetramethoxy-4,4'-bis(diphenylphosphino)-3,3'-bipyridine in butan-1-ol
T=100°C; Suzuki coupling; 20 h; Inert atmosphere;
参考文献
Fu, Xing-Li; Wu, Lei-Lei; Fu, Hai-Yan; Chen, Hua; Li, Rui-Xiang
European Journal of Organic Chemistry, 2009 , # 13 p. 2051 - 2054
反应条件
1: 40 percent / sodium carbonate / Pd(PPh3)4 / toluene; ethanol / Heating
2: 13 percent / (o-Tol)3P; NEt3 / Pd(OAc)2 / acetonitrile / 20 h / 125 °C
View Scheme
参考文献
Karig, Gunter; Moon, Maria-Teresa; Thasana, Nopporn; Gallagher, Timothy
Organic Letters, 2002 , vol. 4, # 18 p. 3115 - 3118
反应条件
1: 40 percent / sodium carbonate / Pd(PPh3)4 / toluene; ethanol / Heating
2: 13 percent / (o-Tol)3P; NEt3 / Pd(OAc)2 / acetonitrile / 20 h / 125 °C
View Scheme
参考文献
Karig, Gunter; Moon, Maria-Teresa; Thasana, Nopporn; Gallagher, Timothy
Organic Letters, 2002 , vol. 4, # 18 p. 3115 - 3118
