6,7-二甲氧基-4-甲基香豆素合成路线 (共 13 条)
反应条件
2,2'-azo-bisisobutyronitrile; poly(phenylsilane) in benzene-d6 T=82 - 85°C; 3 h; sealed;
参考文献
Chatgilialoglu; Ferreri; Vecchi; Lucarini; Pedulli
Journal of Organometallic Chemistry, 1997 , vol. 545-546, p. 475 - 481
反应条件
potassium carbonate in acetone 8 h; Reflux;
参考文献
Grant, Julie-Ann A.; Bonnick, Tamicka; Gossell-Williams, Maxine; Clayton, Terry; Cook, James M.; Jackson, Yvette A.
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 2 p. 909 - 921
反应条件
sodium hydride in dimethyl sulfoxide T=25°C; 17 h; NaH : pyrocatechlol 3.0; Yields of byproduct given;
参考文献
Kessar, Satinder V.; Gupta, Yash P.; Mohammad, Taj; Goyal, Manju; Sawal, Kewal K.
Journal of the Chemical Society, Chemical Communications, 1983 , # 7 p. 400 - 401
反应条件
sodium hydride in dimethyl sulfoxide T=25°C; 17 h; NaH : pyrocatechlol 1.1; Yields of byproduct given;
参考文献
Kessar, Satinder V.; Gupta, Yash P.; Mohammad, Taj; Goyal, Manju; Sawal, Kewal K.
Journal of the Chemical Society, Chemical Communications, 1983 , # 7 p. 400 - 401
反应条件
sodium hydrogencarbonate; acetone
参考文献
Parmar, V. S.; Singh, S.; Boll, P. M.
Magnetic Resonance in Chemistry, 1988 , vol. 26, p. 430 - 433
Title/Abstract Full Text Show Details
Parmar; Singh
Journal of the Indian Chemical Society, 1987 , vol. 64, # 12 p. 745 - 752
反应条件
1: H2SO4 2: K2CO3 / acetone View Scheme
参考文献
Parmar; Singh
Journal of the Indian Chemical Society, 1987 , vol. 64, # 12 p. 745 - 752
反应条件
1: pyridine; aq. NaOH solution; aqueous potassium peroxo disulfate solution / Erwaermen der schwach angesaeuerten Reaktionsloesung mit Natriumsulfit und wss. Salzsaeure 2: acetone; potassium carbonate View Scheme
参考文献
Sawhney et al.
Proceedings - Indian Academy of Sciences, Section A, 1951 , # 33 p. 11,18
反应条件
1: aqueous hydriodic acid; acetic acid anhydride 2: sodium hydrogencarbonate; acetone View Scheme
参考文献
Bhavsar; Desai
Indian Journal of Pharmacy, 1951 , vol. 13, p. 200,203
参考文献
Sawhney et al.
Proceedings - Indian Academy of Sciences, Section A, 1951 , # 33 p. 11,18
反应条件
potassium carbonate; acetone
参考文献
Parikh; Sethna
Journal of the Indian Chemical Society, 1950 , vol. 27, p. 369,373