1,1,1,5,5,5-六氟-2,2,4,4-戊烷四醇合成路线 （共 6 条）
反应条件
sulfuric acid in toluene T=80°C;
参考文献
Central Glass Company, Limited
Patent: US6384286 B1, 2002 ;
Location in patent: Page column 5 ;
参考文献
Petrova; Kurykin
Russian Chemical Bulletin, 2001 , vol. 50, # 1 p. 155 - 156
反应条件
1: With sodium methylate in tert-butyl methyl ether
T=30 - 40°C; 4.5 h;
2: With sulfuric acid in water
T=20 - 60°C; 6 h;
参考文献
Central Glass Company, Limited
Patent: US6384286 B1, 2002 ;
Location in patent: Page column 4 ;
参考文献
Dikarev, Evgeny V.; Zhang, Haitao; Li, Bo
Angewandte Chemie - International Edition, 2006 , vol. 45, # 33 p. 5448 - 5451
反应条件
1: 86.8 percent / NH4OH / H2O; acetone / 1 h / 2 - 5 °C
2: 78.7 percent / conc. HCl / 3 h / Heating
View Scheme
参考文献
Petrova; Kurykin
Russian Chemical Bulletin, 2001 , vol. 50, # 1 p. 155 - 156
参考文献
Haszeldine et al.
Journal of the Chemical Society, 1951 , p. 609,611
