2-烯丙基-1,3-环己二酮合成路线 （共 16 条）
反应条件
potassium hydroxide; hydrazine hydrate
参考文献
Jacobson,M. et al.
Journal of Medicinal Chemistry, 1971 , vol. 14, p. 236 - 239
反应条件
barium dihydroxide in water Ring cleavage;
参考文献
Meyers; Andres, Charles J.; Resek, James E.; Woodall, Charlotte C.; McLaughlin, Maureen A.; Lee, Peter H.; Price, David A.
Tetrahedron, 1999 , vol. 55, # 29 p. 8931 - 8952
反应条件
N-benzyl-trimethylammonium hydroxide in methanol; water
12 h; Ambient temperature;
参考文献
Rajamannar; Palani; Balasubramanian
Synthetic Communications, 1993 , vol. 23, # 22 p. 3095 - 3108
反应条件
tetrakis(triphenylphosphine) palladium(0) in methanol
Heating;
参考文献
Lapitskaya, M. A.; Pivnitskii, K. K.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 9.2 p. 1665 - 1668
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 9 p. 1926 - 1929
反应条件
1: in acetonitrile
T=20°C;
2: With triethylamine in hexane; ethyl acetate
T=20°C; 0.5 h;
参考文献
Zhang, Yang; Raines, Andrew J.; Flowers II, Robert A.
Journal of Organic Chemistry, 2004 , vol. 69, # 19 p. 6267 - 6272
反应条件
1: in acetonitrile
T=20°C;
2: With triethylamine in hexane; ethyl acetate
T=20°C; 0.5 h;
参考文献
Zhang, Yang; Raines, Andrew J.; Flowers II, Robert A.
Journal of Organic Chemistry, 2004 , vol. 69, # 19 p. 6267 - 6272
反应条件
1.1: 1.85 g / Amberlyst H-15; molecular sieves 4 Angstroem / pentane / 48 h
2.1: CTAN / acetonitrile / 20 °C
2.2: 9 percent / Et3N / hexane; ethyl acetate / 0.5 h / 20 °C
View Scheme
参考文献
Zhang, Yang; Raines, Andrew J.; Flowers II, Robert A.
Journal of Organic Chemistry, 2004 , vol. 69, # 19 p. 6267 - 6272
反应条件
potassium carbonate in acetone
T=80°C; 3 h; Inert atmosphere;
参考文献
Gao, Jihong; Simon, Josephine Orso; Rodrigo, Russell; Assoud, Abdeljalil
Journal of Organic Chemistry, 2013 , vol. 78, # 1 p. 48 - 58
反应条件
toluene-4-sulfonic acid in methanol
Reflux;
参考文献
Yu, Binxun; Jiang, Tuo; Quan, Weiguo; Li, Junpeng; Pan, Xinfu; She, Xuegong
Organic Letters, 2009 , vol. 11, # 3 p. 629 - 632
参考文献
Rama Rao; Reddy
Tetrahedron Letters, 1992 , vol. 33, # 28 p. 4061 - 4064
