苯并[b]呋喃-2-甲醛合成路线 (共 56 条)
反应条件
hydrazine hydrate anschliessend mit Kaliumhydroxid;
参考文献
Bisagni et al.
Journal of the Chemical Society, 1955 , p. 3688,3692
反应条件
1: hydrazine hydrate / anschliessend mit Kaliumhydroxid 2: phosphoryl chloride 3: ueber das Hydrazon View Scheme
参考文献
Bisagni et al.
Journal of the Chemical Society, 1955 , p. 3688,3692
反应条件
pyridine; hydroxylamine hydrochloride; acetic anhydride T=85 - 95°C; 2 h;
参考文献
Bobosikova; Clegg; Coles; Dandarova; Hursthouse; Kiss; Krutosikova; Liptaj; Pronayova; Ramsden
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 8 p. 680 - 689
反应条件
1: toluene / 72 h / 110 °C 2: 1 h / 700 °C / 0.01 Torr / flash vacuum pyrolysis View Scheme
参考文献
Chou, Chin-Hsing; Hsueh, Yu-Tan; Wang, Bo-Chi
Journal of the Chinese Chemical Society, 2011 , vol. 58, # 3 p. 301 - 305
反应条件
hydrogenchloride in 1,4-dioxane
参考文献
Guenther, Dieter; Bosse, Dieter
Angewandte Chemie, 1980 , vol. 92, # 2 p. 138
参考文献
Biovitrum AB
Patent: US6465467 B1, 2002 ;
US 6465467 B1
反应条件
1: 86 percent / tetrahydrofuran; diethyl ether / 2 h / 20 °C 2: triphenylsilyl perrhenate / tetrahydrofuran / 0.5 h / -50 °C View Scheme
参考文献
Matsunaga, Nobuyuki; Kaku, Tomohiro; Itoh, Fumio; Tanaka, Toshimasa; Hara, Takahito; Miki, Hiroshi; Iwasaki, Masahiko; Aono, Tetsuya; Yamaoka, Masuo; Kusaka, Masami; Tasaka, Akihiro
Bioorganic and medicinal chemistry, 2004 , vol. 12, # 9 p. 2251 - 2273
反应条件
1: 30 percent / sodium methoxide / methanol / 4 h / -10 °C 2: 91 percent / Rh2(pbf)4 / toluene / 16 h / 40 °C View Scheme
参考文献
Krutosikova, Alzbeta; Dandarova, Miroslava; Bobosik, Vladimir
Collection of Czechoslovak Chemical Communications, 1994 , vol. 59, # 2 p. 473 - 481
反应条件
piperidine; pyridine T=80 - 115°C; 4 h;
参考文献
Obushak, Mykola D.; Pokhodylo, Nazariy T.; Ostapiuk, Yuri V.; Matiychuk, Vasyl S.
Phosphorus, Sulfur and Silicon and the Related Elements, 2008 , vol. 183, # 1 p. 136 - 143
反应条件
1: 90 percent / toluene / 2 h / Heating 2: 92 percent / aq. KOH / 4 h / Heating View Scheme
参考文献
Paizs, Csaba; Katona, Adrian; Retey, Janos
Chemistry - A European Journal, 2006 , vol. 12, # 10 p. 2739 - 2744