9-苄基-9h-嘌呤-6-胺合成路线 （共 43 条）
参考文献
Maki, Yoshifumi; Kameyama, Keiji; Suzuki, Mikio; Sako, Magoichi; Hirota, Kosaku
Journal of Chemical Research, Miniprint, 1984 , # 12 p. 3601 - 3654
参考文献
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, , vol. 13, p. 398
反应条件
tert-Butyl thionitrate; copper dichloride in tetrahydrofuran; acetonitrile T=25°C; 24 h;
参考文献
Kim, Yong Hae
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 74, # 1-4 p. 249 - 260
参考文献
Krueger
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1894 , vol. 18, p. 424,425
反应条件
tert.-butylnitrite in tetrahydrofuran
T=60 - 65°C; 4 h;
参考文献
Nair, Vasu; Chi, Guochen; Uchil, Vinod R.
Patent: US2006/223834 A1, 2006 ;
Location in patent: Page/Page column 22 ;
US 20060223834 A1
反应条件
1: 90 percent / 180 °C
2: 72 percent / N,N-dimethyl-acetamide / 5 h / 50 °C
View Scheme
参考文献
Maki, Yoshifumi; Kameyama, Keiji; Suzuki, Mikio; Sako, Magoichi; Hirota, Kosaku
Journal of Chemical Research, Miniprint, 1984 , # 12 p. 3601 - 3654
反应条件
1: 90 percent / 180 °C
2: 65 percent / N,N-dimethyl-acetamide / 9 h / 70 °C
View Scheme
参考文献
Maki, Yoshifumi; Kameyama, Keiji; Suzuki, Mikio; Sako, Magoichi; Hirota, Kosaku
Journal of Chemical Research, Miniprint, 1984 , # 12 p. 3601 - 3654
反应条件
1: 90 percent / 180 °C
2: 72 percent / N,N-dimethyl-acetamide / 5 h / 50 °C
3: 69 percent / 0.25M NaOH / ethanol / 0.5 h / Ambient temperature
4: 7 percent / 10percent HCl / 2 h / 100 °C
View Scheme
参考文献
Maki, Yoshifumi; Kameyama, Keiji; Suzuki, Mikio; Sako, Magoichi; Hirota, Kosaku
Journal of Chemical Research, Miniprint, 1984 , # 12 p. 3601 - 3654
反应条件
1: 84 percent / N,N-dimethyl-acetamide / 2 h / 50 °C
2: 82 percent / 0.2N aq. NaOH / H2O / 0.25 h / Heating
View Scheme
参考文献
Fujii, Tozo; Saito, Tohru
Chemical & Pharmaceutical Bulletin, 1985 , vol. 33, # 9 p. 3635 - 3644
反应条件
copper(I) oxide; n-Butyl nitrite
Heating;
参考文献
McKenzie, Thomas C.; Epstein, Joseph W.
Journal of Organic Chemistry, 1982 , vol. 47, # 25 p. 4881 - 4884
