(R)-反式-3-羟基-1-碘-1-辛烯合成路线 （共 10 条）
反应条件
lithium amide in tetrahydrofuran; ammonia T=-78°C; other base and conditions; Product distribution;
参考文献
Ito, Takayori; Okamoto, Sentaro; Sato, Fumie
Tetrahedron Letters, 1989 , vol. 30, # 50 p. 7083 - 7086
反应条件
lithium diisopropyl amide in tetrahydrofuran; hexane T=0°C; 0.5 h;
参考文献
Tetrahedron Letters, , vol. 30, # 50 p. 7083 - 7086
反应条件
lithium amide in tetrahydrofuran; ammonia T=-78°C; other base and conditions; Product distribution;
参考文献
Tetrahedron Letters, , vol. 30, # 50 p. 7083 - 7086
反应条件
benzo[1,3,2]dioxaborole; Oxazaborolidine 2 in toluene
T=-78°C; 15 h;
参考文献
Corey; Bakshi
Tetrahedron Letters, 1990 , vol. 31, # 5 p. 611 - 614
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
T=0 - 20°C;
参考文献
Takahashi, Taichi; Watanabe, Hidenori; Kitahara, Takeshi
Heterocycles, 2002 , vol. 58, p. 99 - 104
反应条件
1: 92 percent / imidazole / dimethylformamide / 0 - 20 °C
2: 72 percent / Cp2ZrHCl; I2 / tetrahydrofuran / 20 °C
3: 83 percent / TBAF / tetrahydrofuran / 0 - 20 °C
View Scheme
参考文献
Takahashi, Taichi; Watanabe, Hidenori; Kitahara, Takeshi
Heterocycles, 2002 , vol. 58, p. 99 - 104
反应条件
1: 72 percent / Cp2ZrHCl; I2 / tetrahydrofuran / 20 °C
2: 83 percent / TBAF / tetrahydrofuran / 0 - 20 °C
View Scheme
参考文献
Takahashi, Taichi; Watanabe, Hidenori; Kitahara, Takeshi
Heterocycles, 2002 , vol. 58, p. 99 - 104
反应条件
in acetone
240 h; Ambient temperaturephosphate buffer, pH 7, Lipase PPL;
参考文献
Shimizu, Makoto; Kawanami, Hiroshi; Fujisawa, Tamotsu
Chemistry Letters, 1992 , # 1 p. 107 - 110
反应条件
binaphthol-modified lithium aluminum hydride lt;(S)-6gt;
Yield given. Yields of byproduct given;
参考文献
Suzuki; Kawagishi; Noyori
Tetrahedron Letters, 1982 , vol. 23, # 39 p. 4057 - 4060
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Brieden, Walter; Ostwald, Roswitha; Knochel, Paul
Angewandte Chemie, 1993 , vol. 105, # 4 p. 629 - 631
