1: in acetone
2 h; RefluxInert atmosphere;
2: With zinc in acetone
24 h; RefluxInert atmosphere;
参考文献
Commissariat A L'Energie Atomique; Centre National De La Recherche Scientifique; Universite Pierre Et Marie Curie (Paris 6)
Patent: US2011/83730 A1, 2011 ;
Location in patent: Page/Page column 7 ;
1.1: AlCl3, aluminium chloride / dichloromethane / 24 h / 20 °C / Inert atmosphere; Reflux
2.1: tetraphosphorus decasulfide; lithium perchlorate; acetic acid / 3 h / Reflux
3.1: acetone / 2 h / Reflux; Inert atmosphere
3.2: 24 h / Reflux; Inert atmosphere
View Scheme
参考文献
Commissariat A L'Energie Atomique; Centre National De La Recherche Scientifique; Universite Pierre Et Marie Curie (Paris 6)
Patent: US2011/83730 A1, 2011 ;
1.1: AlCl3, aluminium chloride / dichloromethane / 24 h / 20 °C / Inert atmosphere; Reflux
2.1: tetraphosphorus decasulfide; lithium perchlorate; acetic acid / 3 h / Reflux
3.1: acetone / 2 h / Reflux; Inert atmosphere
3.2: 24 h / Reflux; Inert atmosphere
View Scheme
参考文献
Commissariat A L'Energie Atomique; Centre National De La Recherche Scientifique; Universite Pierre Et Marie Curie (Paris 6)
Patent: US2011/83730 A1, 2011 ;
