(3,3-二甲基-1-丁炔)-苯合成路线 （共 61 条）
参考文献
Sauvetre, R.; Normant, J.F.
Tetrahedron Letters, 1982 , vol. 23, # 42 p. 4325 - 4328
反应条件
n-butyllithium
1.) hexane, THF, -70 deg C, 20 min, 2.) hexane, THF, from -70 deg C to 0 deg C, 2.5 h; Yield given. Multistep reaction;
参考文献
Shioiri, Takayuki; Iwamoto, Yuji; Aoyama, Toyohiko
Heterocycles, 1987 , vol. 26, # 6 p. 1467 - 1470
参考文献
Truce,W.E.; Wolf,G.C.
Journal of Organic Chemistry, 1971 , vol. 36, # 13 p. 1727 - 1732
反应条件
magnesium
1.) Et2O; 2.) 12 h, RT; 2 h, reflux; Yield given. Multistep reaction;
参考文献
Mesnard, Danielle; Bernadou, Francoise; Miginiac, Leone
Journal of Chemical Research, Miniprint, 1981 , # 9 p. 3216 - 3245
反应条件
in dimethyl sulfoxide
T=35 - 40°C; 7 h; Irradiation1.) var. of reaction time; 2.) var. of condition of irradiation; 3.) other PhC<*>CQ substrates with different alkyl or aryl mercury chlorides; 4.) var. concentration, radiation source.; Product distributionMechanism;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha
Tetrahedron Letters, 1986 , vol. 27, # 30 p. 3479 - 3482
反应条件
2,2'-azo-bisisobutyronitrile in acetonitrile
0.7 h; Heating; Yield given. Yields of byproduct given;
参考文献
Gong, Jianchun; Fuchs
Tetrahedron Letters, 1997 , vol. 38, # 5 p. 787 - 790
参考文献
Kauffmann,T.; Sobel,J.
Chemische Berichte, 1966 , vol. 99, p. 1843 - 1850
反应条件
in dichloromethane
T=15°C; 0.166667 h; Irradiationvar. solvents; other iodonium salts; Product distributionQuantum yieldMechanism;
参考文献
Kitamura, Tsugio; Tanaka, Toshimasa; Taniguchi, Hiroshi
Chemistry Letters, 1992 , # 11 p. 2245 - 2248
反应条件
1: With tris-(dibenzylideneacetone)dipalladium(0); tri-cyclo-hexyl-phosphine in 1,4-dioxane
T=20°C; 0.25 h; Inert atmosphere;
2: With formic acid in 1,4-dioxane
T=80°C; Inert atmosphere; stereoselective reaction;
参考文献
Shen, Ruwei; Chen, Tieqiao; Zhao, Yalei; Qiu, Renhua; Zhou, Yongbo; Yin, Shuangfeng; Wang, Xiangbo; Goto, Midori; Han, Li-Biao
Journal of the American Chemical Society, 2011 , vol. 133, # 42 p. 17037 - 17044
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate
参考文献
Eisch,J.J.; Amtmann,R.
Journal of Organic Chemistry, 1972 , vol. 37, p. 3410 - 3415
