(3,3-二甲基-1-丁炔)-苯合成路线 (共 61 条)
反应条件
copper(l) iodide; [Pt(PPh3)4] in N,N-dimethyl-formamide
T=120°C; 15 h;
参考文献
Oh, Chang Ho; Reddy, V. Raghava
Synlett, 2004 , # 12 p. 2091 - 2094
反应条件
copper dichloride in tetrahydrofuran
T=0°C; 1.25 h; Inert atmosphere;
参考文献
Cahiez, Gerard; Gager, Olivier; Buendia, Julien
Angewandte Chemie - International Edition, 2010 , vol. 49, # 7 p. 1278 - 1281
反应条件
in tetrahydrofuran
T=-78°C; Yields of byproduct given;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha
Tetrahedron Letters, 1987 , vol. 28, # 49 p. 6113 - 6116
反应条件
in dimethyl sulfoxide
T=35 - 40°C; 7 h; Irradiation;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.; Pla-Dalmau, Anna; Khanna, Rajive K.
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3530 - 3538
反应条件
in dimethyl sulfoxide
T=35 - 40°C; 24 h; Irradiation;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.; Pla-Dalmau, Anna; Khanna, Rajive K.
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3530 - 3538
反应条件
in dimethyl sulfoxide
T=35 - 40°C; 7 h; Irradiation;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.; Pla-Dalmau, Anna; Khanna, Rajive K.
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3530 - 3538
反应条件
in anhydrous butyl ether; pentane
T=-78°C; 0.25 h; Inert atmosphere; regioselective reaction;
参考文献
Marzo, Leyre; Aleman, Jose; Garcia Ruano, Jose Luis
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 4 p. 403 - 407
反应条件
in tetrahydrofuran; pentane
T=-78°C; Inert atmosphere; regioselective reaction;
参考文献
Marzo, Leyre; Aleman, Jose; Garcia Ruano, Jose Luis
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 4 p. 403 - 407
反应条件
in benzene
T=25°C; Irradiation;
参考文献
Haber, Steffen; Schmitz, Marion; Bergstraesser, Uwe; Hoffmann, Juergen; Regitz, Manfred
Chemistry - A European Journal, 1999 , vol. 5, # 5 p. 1581 - 1589
反应条件
in dimethyl sulfoxide
T=35 - 40°C; 24 h; Irradiation;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.
Organometallics, 1988 , vol. 7, p. 696 - 702