byproducts: boron hydride; High Pressure; under N2; diborane and trihalogen-borane was added to toluene at -130°C, then in a closed autoclave the mixture was heated to 120°C for 90 min; at -195.8°C H2 was removed, at room temp. the residue of trihalogen-borane and diborane were removed;
Muetterties,E.L.
Journal of the American Chemical Society, 1960 , vol. 82, p. 4163 - 4166
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Muetterties
Journal of the American Chemical Society, 1959 , vol. 81, p. 2597
