1,1,2,2-四氟乙基甲醚合成路线 （共 11 条）
参考文献
Yakubovich,A.Ya. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1967 , vol. 37, p. 847 - 852,797 - 801
反应条件
in acetonitrile-D3 T=-78 - 20°C; Title compound not separated from byproducts;
参考文献
Suzuta, Tetsuya; Abe, Takashi; Sekiya, Akira
Journal of Fluorine Chemistry, 2003 , vol. 119, # 1 p. 3 - 8
反应条件
calcium chloride T=200°C; Inert atmosphereAutoclave; Temperature;
参考文献
Central Glass Company ,Limited; Okamoto, Masamune; Imura, Hideaki; Takada, Naoto
Patent: US2013/12740 A1, 2013 ;
Location in patent: Paragraph 0092 ;
反应条件
calcium chloride T=200°C; Inert atmosphereAutoclave;
参考文献
Central Glass Company ,Limited; Okamoto, Masamune; Imura, Hideaki; Takada, Naoto
Patent: US2013/12740 A1, 2013 ;
Location in patent: Paragraph 0092 ;
反应条件
1: With hydrogen fluoride T=175°C; Inert atmosphereAutoclave; 2: With calcium chloride T=160°C; Inert atmosphereAutoclave;
参考文献
Central Glass Company ,Limited; Okamoto, Masamune; Imura, Hideaki; Takada, Naoto
Patent: US2013/12740 A1, 2013 ;
Location in patent: Paragraph 0097; 0100 ;
反应条件
water; fluorinated γ-alumina T=180°C; 0.02 h; Inert atmosphereGas phase; Product distribution / selectivity;
参考文献
Central Glass Company, Limited
Patent: EP2161249 A1, 2010 ;
Location in patent: Page/Page column 6-7 ;
反应条件
SbF5 in neat (no solvent)
参考文献
England, David C.
Journal of Organic Chemistry, 1984 , vol. 49, # 21 p. 4007 - 4008
反应条件
oxygen; CF3O(CF2)2OCF2COOCH3; boron trifluoride T=85°C;
参考文献
3M INNOVATIVE PROPERTIES COMPANY
Patent: WO2009/42853 A2, 2009 ;
Location in patent: Page/Page column 13 ;
反应条件
SbF5 in 1,2-dichloro-ethane
T=25°C; 3 h; Autoclave;
参考文献
LONZA LTD; DRESSEL, Martina; HANSELMANN, Paul; ZARAGOZA DOeRWALD, Florencio
Patent: WO2012/7142 A1, 2012 ;
Location in patent: Page/Page column 12-13 ;
反应条件
calcium chloride
T=200°C; Inert atmosphereAutoclave;
参考文献
Central Glass Company ,Limited; Okamoto, Masamune; Imura, Hideaki; Takada, Naoto
Patent: US2013/12740 A1, 2013 ;
Location in patent: Paragraph 0092 ;
