1-氯-1,2,2-三氟-1,2-二硝基乙烷合成路线 （共 10 条）
反应条件
Na2Cr2O7 in sulfuric acid; acetic acid
ratio of glacial acetic acid:H2SO4=8:3; at 10°C 0.5 h;
参考文献
Park, J. D.; Stefani, A. P.; Crawford, G. H.; Lacher, J. R.
Journal of Organic Chemistry, 1961 , vol. 26, p. 3316 - 3319
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Gmelin Handbook: F: PerFHalOrg.8, 2.4, page 2 - 54
反应条件
iron(III) chloride
at 90°C 24 h; FeCl3 mixed with glas powder;
参考文献
Minnesota Mining and Manufacturing Co.
Patent: US3072705 , 1963 ;
C.A., 1963 , vol. 58, p. 10077
参考文献
Park,J.D. et al.
Journal of Organic Chemistry, 1961 , vol. 26, p. 3319 - 3323
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Gmelin Handbook: F: PerFHalOrg.8, 2.4, page 2 - 54
反应条件
dinitrogen tetraoxide
T=52°C;
参考文献
Purdue Res.Found.
Patent: US2447504 , 1945 ;
参考文献
Gmelin Handbook: F: PerFHalOrg.8, 2.4, page 2 - 54
参考文献
Purdue Research Foundation
Patent: US2447504 , 1948 ;
C.A., 1949 , p. 3024
反应条件
nitrogen(II) oxide; iron(III) chloride
Further byproducts given;
参考文献
Park,J.D. et al.
Journal of Organic Chemistry, 1961 , vol. 26, p. 3319 - 3323
反应条件
at 740-760 Torr in 4 h; molar ratio of O2NCF2CFClONO : O2NCF2CFClNO2= 3-4:1;
参考文献
Bissell,E.R.
Journal of Organic Chemistry, 1961 , vol. 26, p. 5100 - 5103
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Gmelin Handbook: F: PerFHalOrg.8, 2.4, page 2 - 54
反应条件
carbon tetrafluoride; nitrogen(IV) oxide
T=49.65°C; Kinetics; Further Variations:TemperaturesReagents;
参考文献
Romano, Rosana M.; Della Vedova, Carlos O.; Czarnowski, Joanna
Zeitschrift fur Physikalische Chemie, 2002 , vol. 216, # 10 p. 1203 - 1217
参考文献
Bissell,E.R.
Journal of Organic Chemistry, 1961 , vol. 26, p. 5100 - 5103
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Gmelin Handbook: F: PerFHalOrg.8, 2.4, page 2 - 54
