N-叔丁基-4-溴苯甲酰胺合成路线 （共 7 条）
参考文献
Centaur Pharmaceuticals, Inc.
Patent: US5472983 A1, 1995 ;
反应条件
sulfuric acid in acetic acid T=20°C; Ritter reaction; 1.5 h; Inert atmosphere;
参考文献
Milne, Jacqueline E.; Baum, Jean C.
Organic Syntheses, 2012 , vol. 89, p. 519 - 526
反应条件
water; caesium carbonate in acetone T=0°C; 0.333333 h; Schlenk techniqueInert atmosphere;
参考文献
Xia, Zhonghua; Zhu, Qiang
Organic Letters, 2013 , vol. 15, # 16 p. 4110 - 4113
参考文献
Sumitomo Pharmaceuticals Company, Limited
Patent: US6384033 B1, 2002 ;
反应条件
1: hydrofluoroboric acid; sodium nitrite / water / 0.58 h / 0 °C 2: caesium carbonate; water / acetone / 0.33 h / 0 °C / |Schlenk technique; |Inert atmosphere View Scheme
参考文献
Xia, Zhonghua; Zhu, Qiang
Organic Letters, 2013 , vol. 15, # 16 p. 4110 - 4113
反应条件
1: SOCl2 / 2 h / Heating 2: CH2Cl2 / 0.25 h View Scheme
参考文献
Hartmann, Rolf W.; Reichert, Martin
Archiv der Pharmazie, 2000 , vol. 333, # 5 p. 145 - 153
反应条件
scandium tris(trifluoromethanesulfonate) in nitromethane T=170°C; 1 h; Irradiation;
参考文献
Mahalingam; Wu, Xiongyu; Alterman, Mathias
Tetrahedron Letters, 2006 , vol. 47, # 18 p. 3051 - 3053
