4,7,10-三氧-1,13-十三烷二胺合成路线 （共 17 条）
反应条件
hydrogen; Grace 2724 sponge cobalt in tert-butyl methyl ether T=120°C; P=42133 Torr; 5 h; Product distribution / selectivity;
参考文献
AIR PRODUCTS AND CHEMICALS, INC.
Patent: EP1512675 A1, 2005 ;
Location in patent: Page/Page column 4-5; 7 ;
反应条件
hydrogen; Grace 2724 sponge cobalt in methanol T=120°C; P=42133 Torr; 5 h; Product distribution / selectivity;
参考文献
AIR PRODUCTS AND CHEMICALS, INC.
Patent: EP1512675 A1, 2005 ;
Location in patent: Page/Page column 4; 7 ;
反应条件
hydrogen; Grace 2724 sponge cobalt T=125°C; P=47304.6 Torr; 4 h; Product distribution / selectivity;
参考文献
AIR PRODUCTS AND CHEMICALS, INC.
Patent: EP1512675 A1, 2005 ;
Location in patent: Page/Page column 4-5; 7 ;
反应条件
hydrogen; Grace 2724 sponge cobalt in water T=60°C; P=42133 Torr; 4 h; Product distribution / selectivity;
参考文献
AIR PRODUCTS AND CHEMICALS, INC.
Patent: EP1512675 A1, 2005 ;
Location in patent: Page/Page column 3; 6 ;
反应条件
ammonia; nickel T=110°C; P=58840.6 Torr; Hydrogenation;
参考文献
Chekulaeva,I.A. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1967 , p. 1752 - 1754
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1967 , p. 1829 - 1832
反应条件
in methanol-d4 T=20°C; 12 h;
参考文献
Saggiomo, Vittorio; Luening, Ulrich
European Journal of Organic Chemistry, 2008 , # 25 p. 4329 - 4333
反应条件
triethylamine in tetrahydrofuran; methanol T=0 - 20°C; 1.25 h; Inert atmosphere;
参考文献
YALE UNIVERSITY; SPIEGEL, David, A.; JAKOBSCHE, Charles, E.
Patent: WO2013/70688 A1, 2013 ;
Location in patent: Page/Page column 13; 62; 63 ;
反应条件
triethanolamine in tetrahydrofuran; methanol
参考文献
Carpenter JR., Alan P.
Patent: US2004/208823 A1, 2004 ;
参考文献
CHUGAI SEIYAKU KABUSHIKI KAISHA
Patent: EP1082963 A1, 2001 ;
反应条件
1: 75 percent / Et3N / CH2Cl2 / 4 h / 20 °C 2: 91 percent / pyridine / CH2Cl2; acetonitrile / 3.5 h / 20 °C View Scheme
参考文献
Trester-Zedlitz, Michelle; Kamada, Katsuhiko; Burley, Stephen K.; Fenyoe, David; Chait, Brian T.; Muir, Tom W.
Journal of the American Chemical Society, 2003 , vol. 125, # 9 p. 2416 - 2425
