5-甲基-3,4-二氢-1H-2-萘酮合成路线 （共 13 条）
反应条件
sodium hydrogencarbonate; trifluoroacetic acid in dichloromethane
参考文献
Chen, Li; Cheung, Adrian Wai-Hing; Chu, Xin-Jie; Danho, Waleed; Swistok, Joseph; Wang, Yao; Yagaloff, Keith Alan
Patent: US2002/143141 A1, 2002 ;
US 20020143141 A1
反应条件
sodium hydrogencarbonate; trifluoroacetic acid in dichloromethane
参考文献
Chen, Li; Cheung, Adrian W.; Chu, Xin-Jie; Danho, Waleed; Swistok, Joseph; Yagaloff, Keith A.
Patent: US2001/56179 A1, 2001 ;
US 20010056179 A1
反应条件
titanium tetrachloride in dichloromethane T=0 - 20°C; Friedel Crafts reaction; 3 h;
参考文献
Hon, Yung-Son; Devulapally, Rammohan
Tetrahedron Letters, 2009 , vol. 50, # 41 p. 5713 - 5715
反应条件
aluminium trichloride in dichloromethane T=-15°C; Cycloaddition; 1.5 h;
参考文献
Yao; Pollack
Canadian Journal of Chemistry, 1999 , vol. 77, # 5-6 p. 634 - 638
反应条件
trifluoroacetic acid
参考文献
McKervey, M. Anthony; Tuladhar, Sarbajna M.; Twohig, M. Fiona
Journal of the Chemical Society, Chemical Communications, 1984 , # 2 p. 129 - 130
反应条件
1: SOCl2 / CH2Cl2 2: AlCl3 / CH2Cl2 / 1.5 h / -15 °C View Scheme
参考文献
Cordi, Alex A.; Lacoste, Jean-Michel; Le Borgne, Fabrice; Herve, Yolande; Vaysse-Ludot, Lucile; Descombes, Jean-Jacques; Courchay, Christine; Laubie, Michel; Verbeuren, Tony J.
Journal of Medicinal Chemistry, 1997 , vol. 40, # 18 p. 2931 - 2935
反应条件
rhodium (II) acetate in dichloromethane Buchner reaction; Heating;
参考文献
Cheung, Adrian Wai-Hing; Danho, Waleed; Swistok, Joseph; Qi, Lida; Kurylko, Grazyna; Rowan, Karen; Yeon, Mitch; Franco, Lucia; Chu, Xin-Jie; Chen, Li; Yagaloff, Keith
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 1 p. 133 - 137
反应条件
1: SOCl2 / toluene / Heating 2: diethyl ether / 0 - 20 °C 3: Rh(OAc)2 / CH2Cl2 / Heating View Scheme
参考文献
Cheung, Adrian Wai-Hing; Danho, Waleed; Swistok, Joseph; Qi, Lida; Kurylko, Grazyna; Rowan, Karen; Yeon, Mitch; Franco, Lucia; Chu, Xin-Jie; Chen, Li; Yagaloff, Keith
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 1 p. 133 - 137
反应条件
1: diethyl ether / 0 - 20 °C 2: Rh(OAc)2 / CH2Cl2 / Heating View Scheme
参考文献
Cheung, Adrian Wai-Hing; Danho, Waleed; Swistok, Joseph; Qi, Lida; Kurylko, Grazyna; Rowan, Karen; Yeon, Mitch; Franco, Lucia; Chu, Xin-Jie; Chen, Li; Yagaloff, Keith
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 1 p. 133 - 137
反应条件
1: aq. HBr / acetic acid 2: Na, liq. NH3 View Scheme
参考文献
Bey,P.; Ourisson,G.
Bulletin de la Societe Chimique de France, 1968 , p. 2464 - 2468
