N-苄氧羰基-N-甲基-L-缬氨酸合成路线 （共 10 条）
反应条件
sodium hydride in tetrahydrofuran T=20°C; 24 h;
参考文献
Hasuoka, Atsushi; Nishikimi, Yuji; Nakayama, Yutaka; Kamiyama, Keiji; Nakao, Masafumi; Miyagawa, Ken-Ichiro; Nishimura, Osamu; Fujino, Masahiko
Journal of Antibiotics, 2002 , vol. 55, # 3 p. 322 - 336
反应条件
chloro-trimethyl-silane; sodium cyanoborohydride in acetonitrile 0.166667 h; Ambient temperature;
参考文献
Reddy, G. Vidyasagar; Iyengar
Chemistry Letters, 1999 , # 4 p. 299 - 300
反应条件
1: 90 percent / CSA / toluene / Heating 2: Et3SiH; CF3COOH / CH2Cl2 View Scheme
参考文献
Reddy, G. Vidyasagar; Iyengar
Chemistry Letters, 1999 , # 4 p. 299 - 300
参考文献
Hoffmann-La Roche Inc.
Patent: US4250085 A1, 1981 ;
反应条件
lithium hydroxide in tetrahydrofuran
参考文献
Plattner,P.A. et al.
Helvetica Chimica Acta, 1963 , vol. 46, p. 927 - 935
反应条件
2: aq. NaOH / tetrahydrofuran View Scheme
参考文献
Ovchinnikov,Yu.A. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1962 , # 11 p. 1955 - 1961
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1962 , # 11 p. 2046 - 2054
反应条件
1: aq. NaOH / tetrahydrofuran View Scheme
参考文献
Ovchinnikov,Yu.A. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1962 , # 11 p. 1955 - 1961
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1962 , # 11 p. 2046 - 2054
参考文献
Ovchinnikov,Yu.A. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1962 , # 11 p. 1955 - 1961
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1962 , # 11 p. 2046 - 2054
反应条件
1: diethyl ether 2: H2, 12 N HCl / 10percent Pd-C / methanol / 4 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 59, # 9 p. 2437 - 2446
反应条件
hydrogenchloride 4 h; Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 1959 - 1968
