2-[(4-甲基苯基)硫代]乙胺合成路线 （共 8 条）
反应条件
caesium carbonate in acetonitrile
T=50°C; 48 h;
参考文献
Deng, Shixian; Belvedere, Sandro; Yan, Jiaming; Landry, Donald
Patent: US2009/227788 A1, 2009 ;
Location in patent: Page/Page column 20 ;
反应条件
NaOPr in propan-1-ol
6 h; Heating;
参考文献
Ishibashi, Hiroyuki; Uegaki, Masayuki; Sakai, Manami
Synlett, 1997 , vol. 1997, # 8 p. 915 - 916
反应条件
hydrogenchloride
3 h; Heating;
参考文献
Pirl, Joerg N.; Bell, Charles L.; Bauer, Ludwig
Journal of Organic Chemistry, 1982 , vol. 47, # 20 p. 3971 - 3974
反应条件
methanol
T=-10 - -5°C; Hydrierung des Reaktionsprodukts an Raney-Nickel in Methanol;
参考文献
Heath; Lambert
Journal of the Chemical Society, 1947 , p. 1477,1479
反应条件
ethanol
T=80°C; Erhitzen des Reaktionsprodukts mit wss. HCl und Essigsaeure auf 120-130grad;
参考文献
Siefken
Justus Liebigs Annalen der Chemie, 1949 , vol. 562, p. 75,1114
反应条件
1: 89 percent / 3.5 h / 135 - 198 °C / azeotropoic removal of water with benzene
2: 93 percent / 8 N HCl / 3 h / Heating
View Scheme
参考文献
Pirl, Joerg N.; Bell, Charles L.; Bauer, Ludwig
Journal of Organic Chemistry, 1982 , vol. 47, # 20 p. 3971 - 3974
反应条件
ethanol; hydrazine hydrate
anschliessendes Kochen mit wss.-aethanol. HCl;
参考文献
Novelli; Zwaig
Anales de la Asociacion Quimica Argentina (1921-2001), 1944 , vol. 32, p. 89,91
参考文献
Novelli; Zwaig
Anales de la Asociacion Quimica Argentina (1921-2001), 1944 , vol. 32, p. 89,91
