2-羟基-1,2,2-三苯乙酮合成路线 （共 78 条）
反应条件
in tetrahydrofuran
T=-70°C; 0.25 h;
参考文献
Mitchell, Reginald H.; Iyer, Vivekanantan S.
Tetrahedron Letters, 1993 , vol. 34, # 23 p. 3683 - 3686
反应条件
carbon monoxide in tetrahydrofuran
High Pressure; 0.05 mmol Pd compound, 0.1 mmol Ph2Zn, 2.5 ml THF, CO 30 atm (at -50°), stirred at 25°C for 2 h in presence of 0.2 mmol MgClBr,; GC-MS, GC;
参考文献
Yamashita, Hiroshi; Kobayashi, Toshi-aki; Sakakura, Toshiyasu; Tanaka, Masato
Journal of Organometallic Chemistry, 1988 , vol. 356, p. 125 - 132
参考文献
Delacre
Bulletin de la Societe Chimique de France, 1895 , vol. <3> 13, p. 858
反应条件
in benzene
0.5 h; Irradiation; Further byproducts given;
参考文献
Grant, Richard D.; Pinhey, John T.; Rizzardo, Ezio
Australian Journal of Chemistry, 1984 , vol. 37, # 6 p. 1217 - 1229
反应条件
ytterbium
1.) THF, HMPA, RT, 2.) RT, 4 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Hou, Zhaomin; Takamine, Kan; Aoki, Osamu; Shiraishi, Hiroyuki; Fujiwara, Yuzo; Taniguchi, Hiroshi
Journal of Organic Chemistry, 1988 , vol. 53, # 26 p. 6077 - 6084
反应条件
1: AlCl3 / 30 - 40 °C / auf 70grad
2: glacial acetic acid; nitric acid
View Scheme
参考文献
Biltz
Chemische Berichte, 1899 , vol. 32, p. 655
反应条件
1: ligroine; sodium
2: ligroine
View Scheme
参考文献
Acree
American Chemical Journal, 1903 , vol. 29, p. 602
Chemische Berichte, 1904 , vol. 37, p. 2756
反应条件
T=200°C; Verseifung des erhaltenen Benzoeesters mit alkoh.Kalilauge;
参考文献
Gardeur
Chem. Zentralbl., 1897 , vol. 68, # II p. 661
参考文献
Acree
American Chemical Journal, 1903 , vol. 29, p. 602
Chemische Berichte, 1904 , vol. 37, p. 2756
反应条件
air; sodium acetate; dimethyl sulfoxide
参考文献
Sakurai, Hidehiro; Kamiya, Ikuyo; Kitahara, Hiroaki; Tsunoyama, Hironori; Tsukudad, Tatsuya
Synlett, 2009 , # 2 p. 245 - 248
