4-苯基-1,2,4-三唑啉-3,5-二酮合成路线 （共 84 条）
反应条件
in 1,1,2,2-tetrachloroethylene
T=80°C; 2 h;
参考文献
Adam, Waldemar; Cueto, Omar; Lucchi, Ottorino De
Chemische Berichte, 1982 , vol. 115, # 3 p. 1170 - 1177
反应条件
in 1,1,2,2-tetrachloroethylene
T=80°C; 2 h;
参考文献
Adam, Waldemar; Cueto, Omar; Lucchi, Ottorino De
Chemische Berichte, 1982 , vol. 115, # 3 p. 1170 - 1177
反应条件
in ethyl acetate
T=3°C; 2 h;
参考文献
Hunter, Norman Robert; Krawchuk, Bert Paul; Shiloff, Janice Deborah
Canadian Journal of Chemistry, 1982 , vol. 60, p. 835 - 839
反应条件
in benzene
15.5 h; Irradiation; Yield given. Yields of byproduct given;
参考文献
Jones, David W.; Pomfret, Alan
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 2 p. 263 - 267
反应条件
in dichloromethane
T=0°C; 1 h; other diazoalkanes, further 4-substituted 1,2,4-triazole-3,5(4H)-diones; Product distributionMechanism;
参考文献
Izydore, Robert A.; Chapman, John J.; Mitchell, John A.; Cummings, Robert; Jones, George T.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 1415 - 1422
反应条件
in ethyl acetate
T=3°C;
参考文献
Hunter, Norman Robert; Krawchuk, Bert Paul; Shiloff, Janice Deborah
Canadian Journal of Chemistry, 1982 , vol. 60, p. 835 - 839
反应条件
water in ethyl acetate
12 h; Ambient temperature;
参考文献
Izydore, Robert A.; Johnson, Harriette E.; Horton, Ronald T.
Journal of Organic Chemistry, 1985 , vol. 50, # 23 p. 4589 - 4595
反应条件
tert-butyl alcohol in dichloromethane
Ambient temperature;
参考文献
Izydore, Robert A.; Johnson, Harriette E.; Horton, Ronald T.
Journal of Organic Chemistry, 1985 , vol. 50, # 23 p. 4589 - 4595
反应条件
1: 76 percent / NaI, AcOH / acetone / 0.08 h
2: 1.) NaH / 1.) dioxane, 15 min, 2.) dioxane, 30 min
View Scheme
参考文献
Borhani, David W.; Greene, Frederick D.
Journal of Organic Chemistry, 1986 , vol. 51, # 9 p. 1563 - 1570
反应条件
in benzene
T=78°C; in nonnucleophilic or nucleophilic solvent systems; other temp. and time; Product distributionMechanism;
参考文献
Izydore, Robert A.; Johnson, Harriette E.; Horton, Ronald T.
Journal of Organic Chemistry, 1985 , vol. 50, # 23 p. 4589 - 4595
