4-苯基-1,2,4-三唑啉-3,5-二酮合成路线 （共 84 条）
反应条件
tetrabutylammonium (meta)periodate in acetone T=20°C; 0.5 h;
参考文献
Molina, Claudia L.; Chow, Chun P.; Shea, Kenneth J.
Journal of Organic Chemistry, 2007 , vol. 72, # 18 p. 6816 - 6823
反应条件
1: benzene / 20-25 deg C, 2 h; reflux, 2 h 2: KOH / H2O / 2 h 3: anhydrous Na2SO4, N2O4 / CH2Cl2 / 0 °C View Scheme
参考文献
Adam,W.; Carballeira,N.
Journal of the American Chemical Society, 1984 , vol. 106, p. 2874
反应条件
1: KOH / H2O / 2 h 2: anhydrous Na2SO4, N2O4 / CH2Cl2 / 0 °C View Scheme
参考文献
Adam,W.; Carballeira,N.
Journal of the American Chemical Society, 1984 , vol. 106, p. 2874
反应条件
hydrogenchloride; water in methanol T=20°C; 12 h; Inert atmosphere;
参考文献
Ban, Hitoshi; Nagano, Masanobu; Gavrilyuk, Julia; Hakamata, Wataru; Inokuma, Tsubasa; Barbas, Carlos F.
Bioconjugate Chemistry, 2013 , vol. 24, # 4 p. 520 - 532
反应条件
hydrogenchloride; water in methanol T=20°C; 12 h; Inert atmosphere;
参考文献
Ban, Hitoshi; Nagano, Masanobu; Gavrilyuk, Julia; Hakamata, Wataru; Inokuma, Tsubasa; Barbas, Carlos F.
Bioconjugate Chemistry, 2013 , vol. 24, # 4 p. 520 - 532
反应条件
1: atmospheric moisture / storage conditions 2: t-butyl hypochlorite / CH2Cl2 / 0 °C View Scheme
参考文献
Izydore, Robert A.; Chapman, John J.; Mitchell, John A.; Cummings, Robert; Jones, George T.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 1415 - 1422
反应条件
1: chloroform-d1 / 50 °C / Darkness 2: chloroform-d1 / 25 °C / Darkness 3: chloroform-d1 / 50 °C / Darkness View Scheme
参考文献
Roy, Nabarun; Lehn, Jean-Marie
Chemistry - An Asian Journal, 2011 , vol. 6, # 9 p. 2419 - 2425
反应条件
1: chloroform-d1 / 50 °C / Darkness 2: chloroform-d1 / 25 °C / Darkness 3: chloroform-d1 / 50 °C / Darkness View Scheme
参考文献
Roy, Nabarun; Lehn, Jean-Marie
Chemistry - An Asian Journal, 2011 , vol. 6, # 9 p. 2419 - 2425
反应条件
1: chloroform-d1 / 50 °C / Darkness 2: chloroform-d1 / 25 °C / Darkness 3: chloroform-d1 / 50 °C / Darkness View Scheme
参考文献
Roy, Nabarun; Lehn, Jean-Marie
Chemistry - An Asian Journal, 2011 , vol. 6, # 9 p. 2419 - 2425
反应条件
1: chloroform-d1 / 25 °C / Darkness 2: chloroform-d1 / 50 °C / Darkness View Scheme
参考文献
Roy, Nabarun; Lehn, Jean-Marie
Chemistry - An Asian Journal, 2011 , vol. 6, # 9 p. 2419 - 2425
