3,4-二甲氧基-~-硝基苯乙烯合成路线 （共 36 条）
参考文献
Hocquaux; Viel; Brunaud; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 4 p. 331 - 338
参考文献
Rosenmund
Patent: DE244321 ;
反应条件
1.1: LiAlH4 / tetrahydrofuran / 3 h / Heating
2.1: HOBt; DCC / dimethylformamide / 12 h
2.2: 95 percent / dimethylformamide / 12 h
3.1: 85 percent / POCl3 / toluene / 3 h / Heating
View Scheme
参考文献
Sawant, Devesh; Kumar, Rishi; Maulik, Prakas R.; Kundu, Bijoy
Organic Letters, 2006 , vol. 8, # 8 p. 1525 - 1528
反应条件
1: LAH
2: benzene / 0.75 h / Ambient temperature
3: 55.6 percent / FeSO4*7H2O, NH4OH / H2O / 3 h / Heating
4: 43.7 percent / 6 h / 154 °C
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参考文献
Joshi; Chaudhari; Mogera
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 5 p. 431 - 434
反应条件
1: aqueous-alcoholic hydrochloric acid / Electrolysis.bei der elektrolytischen Reduktion an einer Bleikathode
2: NaOH-solution
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参考文献
Kondo; Kondo
Journal fuer Praktische Chemie (Leipzig), 1930 , vol. <2>126, p. 46
Full Text Show Details
Kondo; Kondo
Yakugaku Zasshi, 1928 , vol. 48, p. 57
Chem. Zentralbl., 1928 , vol. 99, # II p. 55
反应条件
1: aqueous-alcoholic hydrochloric acid / Electrolysis.bei der elektrolytischen Reduktion an einer Bleikathode
2: NaOH-solution
3: phosphorus oxychloride; toluene
4: palladium charcoal; water / Hydrogenation
View Scheme
参考文献
Kondo; Kondo
Journal fuer Praktische Chemie (Leipzig), 1930 , vol. <2>126, p. 46
Full Text Show Details
Kondo; Kondo
Yakugaku Zasshi, 1928 , vol. 48, p. 57
Chem. Zentralbl., 1928 , vol. 99, # II p. 55
