3,4-二甲氧基-~-硝基苯乙烯合成路线 （共 36 条）
反应条件
ethylenediamine 4 h; Reflux; Reagent/catalyst;
参考文献
Yang, Jianxin; Dong, Jing; Lue, Xia; Zhang, Qiang; Ding, Wei; Shi, Xiaoxin
Chinese Journal of Chemistry, 2012 , vol. 30, # 12 p. 2827 - 2833
反应条件
ammonium acetate in nitromethane; acetic acid
参考文献
Byk Gulden Lomberg Chemische Fabrik GmbH
Patent: US6121279 A1, 2000 ;
US 6121279 A
Title/Abstract Full Text Show Details
Altana Pharma AG
Patent: US6476025 B1, 2002 ;
US 6476025 B1
反应条件
tert.-butylnitrite; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical in acetonitrile T=50°C; 3 h; stereoselective reaction;
参考文献
Manna, Srimanta; Jana, Sandipan; Saboo, Tapish; Maji, Arun; Maiti, Debabrata
Chemical Communications, 2013 , vol. 49, # 46 p. 5286 - 5288
反应条件
1H-imidazole; iodine in dichloromethane
参考文献
Rokhum, Lalthazuala; Bez, Ghanashyam
Tetrahedron Letters, 2013 , vol. 54, # 40 p. 5500 - 5504
反应条件
1: sodium hydroxide / ethanol; water / 60 °C 2: copper(l) chloride; tert.-butylnitrite / acetonitrile / 80 °C View Scheme
参考文献
Rokade, Balaji V.; Prabhu, Kandikere Ramaiah
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 39 p. 6713 - 6716
反应条件
CaO modified benzyl bromide T=102°C; Henry Nitro Aldol Condensation; 5 h;
参考文献
Tang, Ying; Gu, Xuefan; Meng, Mei; Xu, Jingfang
Research on Chemical Intermediates, 2013 , vol. 39, # 8 p. 3715 - 3725
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / |Reflux 2: dichloromethane / 1 h / 20 °C 3: lithium aluminium tetrahydride / tetrahydrofuran / 6 h / 0 °C / |Inert atmosphere; |Reflux View Scheme
参考文献
Paul; Anand
Journal of Scientific and Industrial Research, 1958 , vol. 17B, p. 219,223
反应条件
1: LiAlH4 2: NaOH / CH2Cl2 View Scheme
参考文献
Silveira, Claudio C.; Bernardi, Carmem R.; Braga, Antonio L.; Kaufman, Teodoro S.
Tetrahedron Letters, 1999 , vol. 40, # 27 p. 4969 - 4972
反应条件
1: LiAlH4; diethyl ether 2: chloral View Scheme
参考文献
Journal of Scientific and Industrial Research, , vol. 17B, p. 219,223
反应条件
1: LiAlH4 2: NaOH / CH2Cl2 3: 61 percent / SnCl4 / CH2Cl2 / -78 deg C -> r.t. 4: 95 percent / REDAL / toluene View Scheme
参考文献
Silveira, Claudio C.; Bernardi, Carmem R.; Braga, Antonio L.; Kaufman, Teodoro S.
Tetrahedron Letters, 1999 , vol. 40, # 27 p. 4969 - 4972
