1-氯-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十六氟辛烷合成路线 （共 15 条）
423-53-01-氯-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十六氟辛烷
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反应条件
hydrazine hydrate; zinc in N,N-dimethyl-formamide T=70°C; 2 h;
参考文献
Wu, Fang-Hong; Huang, Bing-Nan; Huang, Wei-Yuan
Journal of Fluorine Chemistry, 1995 , vol. 73, # 2 p. 159 - 160
423-53-01-氯-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十六氟辛烷
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反应条件
1: antimony (V)-fluoride / 200 °C 2: chlorine / 100 - 150 °C / im Licht 3: antimony (V)-fluoride / 175 °C View Scheme
参考文献
Kinetic Chem. Inc.
Patent: US2490764 , 1945 ;
423-53-01-氯-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十六氟辛烷
→
参考文献
Kinetic Chem. Inc.
Patent: US2490764 , 1945 ;
423-53-01-氯-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十六氟辛烷
→
反应条件
chlorine; nitrogen(IV) oxide T=600°C; im Nickel-Rohr und Behandeln des Reaktionsprodukts mit wss.Schwefelsaeure;
参考文献
Severson; Brice
Journal of the American Chemical Society, 1958 , vol. 80, p. 2313,2316
423-53-01-氯-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十六氟辛烷+
→
反应条件
beim Leiten durch ein auf 600grad erhitztes Nickelrohr und Behandeln des Reaktionsprodukts mit wss. Schwefelsaeure;
参考文献
Severson; Brice
Journal of the American Chemical Society, 1958 , vol. 80, p. 2313,2316
423-53-01-氯-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十六氟辛烷
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307-33-51-氯-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-十七氟辛烷
反应条件
NiF2; fluorine T=160°C;
参考文献
Zakharov, V. Yu.; Denisov, A. K.; Novikova, M. D.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 12 p. 1942 - 1945
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 12 p. 1844 - 1846
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423-53-01-氯-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十六氟辛烷+
反应条件
[Co(HDm)2Py]Br; zinc in ethanol
T=15°C; 1 h;
参考文献
Hu, Chan-Ming; Qiu, Yao-Ling
Journal of Organic Chemistry, 1992 , vol. 57, # 12 p. 3339 - 3342
→
423-53-01-氯-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十六氟辛烷+
反应条件
[Co(HDm)2Py]Br; zinc in ethanol
T=30°C; 3 h;
参考文献
Hu, Chan-Ming; Qiu, Yao-Ling
Journal of Organic Chemistry, 1992 , vol. 57, # 12 p. 3339 - 3342
→
423-53-01-氯-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十六氟辛烷+
反应条件
[Co(HDm)2Py]Br; zinc in ethanol
T=30°C; 4 h;
参考文献
Hu, Chan-Ming; Qiu, Yao-Ling
Journal of Organic Chemistry, 1992 , vol. 57, # 12 p. 3339 - 3342
→
423-53-01-氯-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十六氟辛烷+
反应条件
[Co(HDm)2Py]Br; zinc in ethanol
T=15°C; 1 h;
参考文献
Hu, Chan-Ming; Qiu, Yao-Ling
Journal of Organic Chemistry, 1992 , vol. 57, # 12 p. 3339 - 3342
