2,2,3,3,4,4,5-七氟-5-(七氟丙基)四氢呋喃合成路线 (共 9 条)
反应条件
cobalt(III) fluoride
T=440°C;
参考文献
Chambers, Richard D.; Grievson, Brian
Journal of Fluorine Chemistry, 1984 , vol. 25, p. 523 - 534
反应条件
fluorspar; cobalt(III) fluoride
T=440°C; in nickel tube; var. temp.;
参考文献
Chambers, Richard D.; Grievson, Brian; Drakesmith, Frederick G.; Powell, Richard L.
Journal of Fluorine Chemistry, 1985 , vol. 29, p. 323 - 340
反应条件
hydrogen fluoride
T=5 - 6°C; 6.81667 h; electrochemical cell; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Abe, Takashi; Hayashi, Eiji; Baba, Hajime; Kodaira, Kazuo; Nagase, Shunji
Journal of Fluorine Chemistry, 1980 , vol. 15, p. 353 - 380
反应条件
hydrogen fluoride
T=5 - 6°C; 6.55 h; electrochemical fluorination; anodic current density 3.5 A/dm2, 5.3 - 8.5 V; Yield given. Further byproducts given;
参考文献
Abe,T.; Baba,H.; Hayashi,E.
Journal of Fluorine Chemistry, 1983 , vol. 23, p. 123
反应条件
hydrogen fluoride
T=5 - 6°C; 6.81667 h; electrochemical cell; Further byproducts given. Yields of byproduct given;
参考文献
Abe, Takashi; Hayashi, Eiji; Baba, Hajime; Kodaira, Kazuo; Nagase, Shunji
Journal of Fluorine Chemistry, 1980 , vol. 15, p. 353 - 380
反应条件
hydrogen fluoride
T=5 - 6°C; 6.55 h; electrochemical fluorination; anodic current density 3.5 A/dm2, 5.3 - 8.5 V; Further byproducts given;
参考文献
Abe,T.; Baba,H.; Hayashi,E.
Journal of Fluorine Chemistry, 1983 , vol. 23, p. 123
反应条件
hydrogen fluoride
T=5 - 6°C; 6.55 h; electrochemical fluorination; anodic current density 3.5 A/dm2, 5.3 - 8.5 V; Further byproducts given;
参考文献
Abe,T.; Baba,H.; Hayashi,E.
Journal of Fluorine Chemistry, 1983 , vol. 23, p. 123
反应条件
hydrogen fluoride
T=5 - 6°C; 6.81667 h; electrochemical fluorination of various 2-alkyl substituted oxanes; Product distribution;
参考文献
Abe, Takashi; Hayashi, Eiji; Baba, Hajime; Kodaira, Kazuo; Nagase, Shunji
Journal of Fluorine Chemistry, 1980 , vol. 15, p. 353 - 380
反应条件
hydrogen fluoride
6.55 h; electrochemical fluorination; anodic current density 3.5 A/dm2, 5.3 -8 .5 V; products passed on NaF; Product distribution;
参考文献
Abe,T.; Baba,H.; Hayashi,E.
Journal of Fluorine Chemistry, 1983 , vol. 23, p. 123