2-乙酰氨基-1-氨基-1,2-二脱氧-beta-D-吡喃葡萄糖合成路线 （共 12 条）
反应条件
palladium 10 on activated carbon; hydrogen in methanol T=20°C; 2 h;
参考文献
Joseph, Ryan; Dyer, Frank Brock; Garner, Philip
Organic Letters, 2013 , vol. 15, # 4 p. 732 - 735
反应条件
anhydrous ammonium carbonate
参考文献
Meldal, Morten; Book, Klaus
Tetrahedron Letters, 1990 , vol. 31, # 48 p. 6987 - 6990
反应条件
ammonium hydrogen carbonate T=42°C; 36 h;
参考文献
Shin, Injae; Jung, Hyuk-Jun; Lee, Myung-Ryul
Tetrahedron Letters, 2001 , vol. 42, # 7 p. 1325 - 1328
反应条件
1: 92 percent / ammonia / methanol / 24 h / Ambient temperature 2: 88 percent / hydrogen / PtO2 (Adam's catalyst) / methanol / 3 h View Scheme
参考文献
Joseph, Ryan; Dyer, Frank Brock; Garner, Philip
Organic Letters, 2013 , vol. 15, # 4 p. 732 - 735
反应条件
1.1: 20 °C 2.1: sodium azide / N,N-dimethyl-formamide / 70 °C 3.1: magnesium; methanol / 3 h / 20 °C / |Inert atmosphere 3.2: Amberlyst 15 ion exchange resin / 0.17 h / 20 °C / |Inert atmosphere 4.1: hydrogen; palladium 10 on activated carbon / methanol / 2 h / 20 °C View Scheme
参考文献
Joseph, Ryan; Dyer, Frank Brock; Garner, Philip
Organic Letters, 2013 , vol. 15, # 4 p. 732 - 735
反应条件
1.1: sodium azide / N,N-dimethyl-formamide / 70 °C 2.1: magnesium; methanol / 3 h / 20 °C / |Inert atmosphere 2.2: Amberlyst 15 ion exchange resin / 0.17 h / 20 °C / |Inert atmosphere 3.1: hydrogen; palladium 10 on activated carbon / methanol / 2 h / 20 °C View Scheme
参考文献
Joseph, Ryan; Dyer, Frank Brock; Garner, Philip
Organic Letters, 2013 , vol. 15, # 4 p. 732 - 735
反应条件
1.1: sodium methylate / methanol 1.2: 0 - 20 °C 2.1: 20 °C 3.1: sodium azide / N,N-dimethyl-formamide / 70 °C 4.1: magnesium; methanol / 3 h / 20 °C / |Inert atmosphere 4.2: Amberlyst 15 ion exchange resin / 0.17 h / 20 °C / |Inert atmosphere 5.1: hydrogen; palladium 10 on activated carbon / methanol / 2 h / 20 °C View Scheme
参考文献
Joseph, Ryan; Dyer, Frank Brock; Garner, Philip
Organic Letters, 2013 , vol. 15, # 4 p. 732 - 735
反应条件
1: methanol 2: 61 percent / NBS; H2O / acetone 3: NH4HCO3 View Scheme
参考文献
Wang, Zhi-Guang; Zhang, XuFang; Live, David; Danishefsky, Samuel J.
Angewandte Chemie (International Edition in English), 2000 , vol. 39, # 20 p. X3652-3656
反应条件
1.1: bisdicollidine iodonium perchloride 1.2: 68 percent / LiHMDS 2.1: Na; NH3 3.1: methanol 4.1: 61 percent / NBS; H2O / acetone 5.1: NH4HCO3 View Scheme
参考文献
Wang, Zhi-Guang; Zhang, XuFang; Live, David; Danishefsky, Samuel J.
Angewandte Chemie (International Edition in English), 2000 , vol. 39, # 20 p. X3652-3656
反应条件
1: Na; NH3 2: methanol 3: 61 percent / NBS; H2O / acetone 4: NH4HCO3 View Scheme
参考文献
Wang, Zhi-Guang; Zhang, XuFang; Live, David; Danishefsky, Samuel J.
Angewandte Chemie (International Edition in English), 2000 , vol. 39, # 20 p. X3652-3656
