5-甲基-4-己烯-1-醇合成路线 （共 44 条）
参考文献
Schneider; Cloux; Foti; Kovats
Synthesis, 1990 , # 11 p. 1027 - 1031
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Schneider; Cloux; Foti; Kovats
Synthesis, 1990 , # 11 p. 1027 - 1031
反应条件
1-ethyl-3-methylimidazolium trifluoromethanesulfonate; ytterbium(III) triflate T=120°C; Inert atmosphere; regioselective reaction;
参考文献
Dzudza, Alma; Marks, Tobin J.
Chemistry - A European Journal, 2010 , vol. 16, # 11 p. 3403 - 3422
反应条件
1: pyridinium chlorochromate / CH2Cl2 / 2 h / Ambient temperature 2: diethyl ether View Scheme
参考文献
Marfat,A. et al.
Journal of Organic Chemistry, 1979 , vol. 44, # 22 p. 3888 - 3901
反应条件
1: pyridinium chlorochromate / CH2Cl2 / 2 h / Ambient temperature 2: diethyl ether View Scheme
参考文献
Marfat,A. et al.
Journal of Organic Chemistry, 1979 , vol. 44, # 22 p. 3888 - 3901
反应条件
1: 1.) toluene-p-sulphonyl chloride,pyridine, 2.) sodium iodide / 1.) 24 h, 2.) acetone, reflux, 16 h
2: 24 g
3: water, silver oxide / 15 °C
4: 150 - 160 °C
View Scheme
参考文献
Cocker, Wesley; Geraghty, Niall W. A.; McMurry, T. Brian H.; Shannon, Patrick V. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 10 p. 2245 - 2254
反应条件
aluminum isopropoxide
T=70 - 120°C; Erhitzen unter vermindertem Druck und folgenden Einleiten von Zimtaldehyd unter 21 mm bei 140-160grad;
参考文献
Lee; Hur; Park
Tetrahedron Letters, 1989 , vol. 30, # 51 p. 7219 - 7220
反应条件
pyridine; tert-butylhypochlorite in dichloromethane
Ambient temperatureother Δ4-alkenols;
参考文献
Konstantinovic, S.; Bugarcic, Z.; Milovanovic, J. N.; Mihailovic, M. Lj.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 4 p. 354 - 356
反应条件
triethylamine in dichloromethane
参考文献
Curran, Dennis P.; Yu, Hosung; Liu, Hongtao
Tetrahedron, 1994 , vol. 50, # 25 p. 7343 - 7366
反应条件
1: 81 percent / pyridine / 0 °C
2: 80 percent / 2.) 10 percent aq. NaOH / Heating
3: 84 percent / nitrosation
4: 67 percent / LiAlH4
5: 25 percent / HgO
View Scheme
参考文献
Newcomb,M.; Burchill,Mt.; Deeb,T.M.
Journal of the American Chemical Society, 1988 , vol. 110, p. 6528
