5-甲基-4-己烯-1-醇合成路线 （共 44 条）
反应条件
potassium tert-butylate in tetrahydrofuran
参考文献
Corey; Cheng, Hengmiao; Baker, C. Hunter; Matsuda, Seiichi P. T.; Li, Ding; Song, Xuelei
Journal of the American Chemical Society, 1997 , vol. 119, # 6 p. 1277 - 1288
反应条件
potassium hydroxide; lithium aluminium tetrahydride Multistep reaction;
参考文献
Mori, Kenji; Sugai, Takeshi; Maeda, Yukari; Okazaki, Tomomi; Noguchi, Tadashi; Naito, Hiroshi
Tetrahedron, 1985 , vol. 41, # 22 p. 5307 - 5312
反应条件
1: 76 percent / H3PO4 / 2 h / 150 °C / 3800 Torr 2: 74 percent / NaBH4 / H2O / 50 deg C -> 30 deg C View Scheme
参考文献
Yonova, Ivelina M.; Johnson, A. George; Osborne, Charlotte A.; Moore, Curtis E.; Morrissette, Naomi S.; Jarvo, Elizabeth R.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 9 p. 2422 - 2427
Angew. Chem., 2014 , vol. 126, # 9 p. 2454 - 2459,6
反应条件
2: 1.) KOH 2.) LiAlH4 View Scheme
参考文献
Mori, Kenji; Sugai, Takeshi; Maeda, Yukari; Okazaki, Tomomi; Noguchi, Tadashi; Naito, Hiroshi
Tetrahedron, 1985 , vol. 41, # 22 p. 5307 - 5312
反应条件
1,1,1,2,2,2-hexabutyl-distannane in benzene Irradiation;
参考文献
Keck, Gary E.; Byers, Jeffrey H.
Journal of Organic Chemistry, 1985 , vol. 50, # 25 p. 5442 - 5444
反应条件
1: 81 percent / 1.) NaH / tetrahydrofuran / 1.) 0 deg C, 30 min; 2.) RT, 2 h 2: 95 percent / LiCl, H2O / dimethylsulfoxide / 5 h / Heating 3: 56 percent / LiAlH4 / tetrahydrofuran View Scheme
参考文献
Cane, David E.; Tandon, Manish
Tetrahedron Letters, 1994 , vol. 35, # 30 p. 5355 - 5358
反应条件
copper(l) iodide in tetrahydrofuran
参考文献
Linstrumelle,G. et al.
Tetrahedron Letters, 1978 , p. 4069 - 4072
反应条件
(i) Mg, (ii) /BRN= 1209228/; Multistep reaction;
参考文献
Franke, L.R. Rodriguez-Avial; Wolf, H.; Wray, V.
Tetrahedron, 1984 , vol. 40, # 18 p. 3491 - 3498
反应条件
1: tetrahydrofuran-2-one With diisobutylaluminium hydride 2: isopropyl-triphenyl-phosphonium iodide Wittig reaction; Further stages.;
参考文献
Boyer, Francois-Didier; Hanna, Issam
Organic Letters, 2007 , vol. 9, # 12 p. 2293 - 2295
反应条件
1: 11.7 g / pyridine / H2O / 2 h / Heating 2: 18.4 g / lithium aluminium hydride / diethyl ether / 1.) 0 deg C, 2.) reflux, 1 h View Scheme
参考文献
Cocker, Wesley; Geraghty, Niall W. A.; McMurry, T. Brian H.; Shannon, Patrick V. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 10 p. 2245 - 2254
