(R)-噻唑烷-4-甲酸甲酯合成路线 (共 10 条)
反应条件
manganese(IV) oxide in benzene T=60°C; 6 h;
参考文献
Iwakawa, Masaharu; Kobayashi, Yasunobu; Ikuta, Shun-ichi; Yoshimura, Juji
Chemistry Letters, 1982 , p. 1975 - 1978
反应条件
triethylamine in dichloromethane
T=20°C;
参考文献
Selambarom, Jimmy; Carre, Francis; Fruchier, Alain; Roque, Jean Pierre; Pavia, Andre A
Tetrahedron, 2002 , vol. 58, # 22 p. 4439 - 4444
反应条件
potassium carbonate in dichloromethane
T=20°C; 24 h;
参考文献
Braga, Antonio Luiz; Milani, Priscila; Vargas, Fabricio; Paixao, Marcio W.; Sehnem, Jasquer A.
Tetrahedron Asymmetry, 2006 , vol. 17, # 19 p. 2793 - 2797
反应条件
thionyl chloride
1.) -20 deg C, 30 min, 2.) RT, 6 h;
参考文献
Aitken, R. Alan; Mesher, Shaun T. E.
Journal of Chemical Research, Miniprint, 1998 , # 2 p. 564 - 579
反应条件
triethylamine in dichloromethane
T=20°C;
参考文献
Selambarom, Jimmy; Smadja, Jacqueline; Pavia, Andre A.
Tetrahedron Letters, 2005 , vol. 46, # 4 p. 615 - 617
参考文献
Ratner; Clarke
Journal of the American Chemical Society, 1937 , vol. 59, p. 200,201, 205
参考文献
Iwakawa, Masaharu; Kobayashi, Yasunobu; Ikuta, Shun-ichi; Yoshimura, Juji
Chemistry Letters, 1982 , p. 1975 - 1978
参考文献
Northrop,R.C.; Russ,P.L.
Journal of Organic Chemistry, 1975 , vol. 40, p. 558 - 559
反应条件
hydrogenchloride
1.) water, 20 h, 2.) reflux, 6 h; Yield given. Multistep reaction;
参考文献
Beagley, Brian; Betts, Michael J.; Pritchard, Robin G.; Schofield, Anthony; Stoodley, Richard J.; Vohra, Shaheen
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , p. 1761 - 1770
参考文献
Takata, Toshikazu; Kuo, Mingjung; Tamura, Yoshiharu; Kabe, Yoshio; Ando, Wataru
Chemistry Letters, 1985 , p. 939 - 942