1-(4-甲基苯基)-3-苯基丙-2-烯-1-酮合成路线 (共 63 条)
反应条件
sulfuric acid; acetic acid; ruthenium trichloride T=24.85 - 39.85°C; Catalytic oxidation; Kinetics;
参考文献
Annapoorna; Prasad Rao; Sethuram
International Journal of Chemical Kinetics, 2000 , vol. 32, # 10 p. 581 - 588
反应条件
sulfuric acid; mercury(II) diacetate; bromate anion in water; acetic acid T=26.9°C; Eexp., ΔH(excit.), ΔS(excit.), ΔG(excit.); MechanismRate constantThermodynamic data;
参考文献
Char, P. Narasimha; Sondu, S.; Sethuram, B.; Rao, T. Navaneeth
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1987 , vol. 26, # 9 p. 749 - 751
反应条件
1,1'-bis(di-tert-butylphosphino)ferrocene palladium dichloride; potassium carbonate in 1,4-dioxane
T=140°C; 0.5 h; Inert atmosphereMicrowave irradiation;
参考文献
Al-Masum, Mohammad; Ng, Eunice; Wai, Maya Chen
Tetrahedron Letters, 2011 , vol. 52, # 9 p. 1008 - 1010
反应条件
zinc oxide
T=25 - 30°C; Friedel-Crafts Acylation; 0.25 h; regioselective reaction;
参考文献
More, Parmeshwar E.; Bandgar, Babasaheb P.; Kamble, Vinod T.
Catalysis Communications, 2012 , vol. 27, p. 30 - 32
反应条件
PEG400; sodium hydroxide in water
T=20°C; aldol condensation; 24 h;
参考文献
Krishnakumar; Swaminathan
Journal of Molecular Catalysis A: Chemical, 2011 , vol. 350, # 1-2 p. 16 - 25
反应条件
sodium tetrahydroborate; nickel dichloride in methanol
T=20°C; 0.583333 h;
参考文献
Khurana, Jitender M.; Kandpal, Bhaskar M.; Kukreja, Gagan; Sharma, Purnima
Canadian Journal of Chemistry, 2006 , vol. 84, # 8 p. 1019 - 1023
反应条件
[Pd(η3-1-Ph-allyl)(μ-Cl)]2; 1,3-bis-(diphenylphosphino)propane; triethylamine in toluene
T=100°C; carbonylative Heck reaction; P=7500.75 Torr; 20 h; Autoclave;
参考文献
Wu, Xiao-Feng; Neumann, Helfried; Beller, Matthias
Angewandte Chemie - International Edition, 2010 , vol. 49, # 31 p. 5284 - 5288
反应条件
[Ir2(COD)2(SnCl3)2(Cl)2(μ-Cl)2] in 1,2-dichloro-ethane
T=80°C; 0.75 h; Inert atmosphere;
参考文献
Chatterjee, Paresh Nath; Roy, Sujit
Tetrahedron, 2012 , vol. 68, # 19 p. 3776 - 3785
反应条件
1-benzyl-1-aza-4-azoniabicyclolt;2.2.2gt;octane periodate in acetonitrile
40 h; Heating;
参考文献
Hajipour, A. R.; Mahboobkhah, N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1998 , vol. 37, # 3 p. 285 - 287
反应条件
samarium (III) iodide in tetrahydrofuran
T=20°C; 3 h;
参考文献
Fan, Xuesen; Zhang, Yongmin
Journal of Chemical Research - Part S, 2002 , # 9 p. 439 - 441