3-(4-甲基苯基)-1-苯基-丙-2-烯-1-酮合成路线 (共 36 条)
反应条件
1: 88 percent / sodium acetate / ethanol; H2O / 1 h / Heating 2: 88 percent / HCl / 1 h / Heating 3: 70 percent / 5percent bromine water / H2O / 2 h View Scheme
参考文献
Soliman; Faid-Allah; El Sadany
Journal of Pharmaceutical Sciences, 1987 , vol. 76, # 8 p. 626 - 632
参考文献
Robert; Hassanine; Harraga; Seilles
Annales Pharmaceutiques Francaises, 1995 , vol. 53, # 6 p. 261 - 271
反应条件
acetic acid T=20°C; 1.5 h; Sonication;
参考文献
Lin, Zhi-Ping; Li, Ji-Tai
E-Journal of Chemistry, 2012 , vol. 9, # 1 p. 267 - 271
反应条件
1: With C20H24F6MnN4O6S2 in acetonitrile T=20°C; 0.05 h; Inert atmosphere; 2: With peracetic acid in acetonitrile T=20°C; 1.33333 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Wang, Bin; Miao, Cheng-Xia; Wang, Shou-Feng; Kuehn, Fritz E.; Xia, Chun-Gu; Sun, Wei
Journal of Organometallic Chemistry, 2012 , vol. 715, p. 9 - 12
反应条件
sodium hydroxide; C55H69F12N7O2*ClH; dihydrogen peroxide in water; toluene T=-10°C; 4 h; Inert atmosphere; optical yield given as percent ee;
参考文献
Tanaka, Shinji; Nagasawa, Kazuo
Synlett, 2009 , # 4 p. 667 - 670
反应条件
hydroxylamine hydrochloride; [N-butylthiazolium][Br] T=20°C; 0.833333 h; Ionic liquid;
参考文献
Safaei-Ghomi, Javad; Ghasemzadeh, Mohammad Ali
Journal of the Serbian Chemical Society, 2012 , vol. 77, # 6 p. 733 - 739
反应条件
1: 59 percent / CH2Cl2 / 40 - 42 °C 2: 60 percent / KOH / ethanol / Heating View Scheme
参考文献
Prakash, Om; Kumar, Rajesh; Sharma, Deepak; Pannu, Kamaljeet; Kamal, Raj
Synlett, 2007 , # 14 p. 2189 - 2192
反应条件
potassium hydroxide in tert-butyl alcohol T=40 - 50°C; Corey-Chaykovsky epoxidation; 12 h;
参考文献
Letters in Organic Chemistry, , vol. 8, # 7 p. 509 - 514
反应条件
sulfuric acid; periodate(1-); ruthenium(III) cation in acetic acid T=50°C; MechanismRate constant;
参考文献
Annapoorna; Prasad Rao; Sethuram
International Journal of Chemical Kinetics, 2000 , vol. 32, # 10 p. 581 - 588
反应条件
sodium ethanolate in neat (no solvent) Michael Addition; 0.0333333 h; Microwave irradiationGreen chemistry;
参考文献
Paul, Nidhin; Shanmugam, Muniyappapillai Jeganathan; Muthusubramanian, Shanmugam
Synthetic Communications, 2013 , vol. 43, # 1 p. 129 - 138