2-(溴甲基)丙烯酸甲酯合成路线 （共 27 条）
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=25°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Giri, Somnath
European Journal of Organic Chemistry, 2012 , # 24 p. 4580 - 4589
反应条件
palladium (II) trifluoroacetate; potassium hydroxide in water T=90°C; Suzuki Coupling; Green chemistry;
参考文献
Dong, Chaonan; Zhang, Lingjuan; Xue, Xiao; Li, Huanrong; Yu, Zhiyong; Tang, Weijun; Xu, Lijin
RSC Advances, 2014 , vol. 4, # 22 p. 11152 - 11158
反应条件
chloro-trimethyl-silane; ethylene dibromide; lithium chloride; zinc
参考文献
Quan, Mimi L.; Ellis, Christopher D.; Liauw, Ann Y.; Alexander, Richard S.; Knabb, Robert M.; Lam, Gilbert; Wright, Matthew R.; Wong, Pancras C.; Wexler, Ruth R.
Journal of Medicinal Chemistry, 1999 , vol. 42, # 15 p. 2760 - 2773
反应条件
1-hydroxybut-2-yne; nickel(0)tetracarbonyl in acetone T=30°C; 12 h;
参考文献
Camps, Francisco; Moreto, Josep M.; Pages, Lluis
Tetrahedron, 1992 , vol. 48, # 15 p. 3147 - 3162
反应条件
lead(II) bromide; aluminium in water; N,N-dimethyl-formamide 10 h; Ambient temperature;
参考文献
Tanaka, Hideo; Yamashita, Shiro; Toru, Sigeru
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, p. 1951 - 1953
反应条件
in acetone T=30°C; 12 h;
参考文献
Camps, Francisco; Moreto, Josep M.; Pages, Lluis
Tetrahedron, 1992 , vol. 48, # 15 p. 3147 - 3162
反应条件
1,4-diaza-bicyclo[2.2.2]octane T=20°C; Baylis-Hillman reaction; 168 h;
参考文献
Basavaiah, Deevi; Sharada, Duddu S.; Kumaragurubaran, Nagaswamy; Reddy, Ravi Mallikarjuna
Journal of Organic Chemistry, 2002 , vol. 67, # 20 p. 7135 - 7137
反应条件
1: 1) iPr2NH, n-BuLi / 1) THF, -78 deg C, 30 min, 2) HMPA, 25 deg C 2: methanol / 25 °C 3: DBN / benzene / Heating View Scheme
参考文献
Grigg, Ronald; Dorrity, Michael J.; Heaney, Frances; Malone, John F.; Rajviroongit, Shuleewan; Sridharan, Visuvanathar; Surendrakumar, Sivagnanasundram
Tetrahedron, 1991 , vol. 47, # 38 p. 8297 - 8322
反应条件
1: With bis(η5-cyclopentadienyl)titanium dichloride in tetrahydrofuran
T=20°C; 5 h;
2: With sulfuric acid in tetrahydrofuran
7 h;
参考文献
Paira, Moumita; Banerjee, Biplab; Jana, Samaresh; Mandal, Samir Kumar; Roy, Subhas Chandra
Tetrahedron Letters, 2007 , vol. 48, # 18 p. 3205 - 3207
反应条件
zinc dibromide in dichloromethane
Ambient temperature;
参考文献
Morrow, Gregory R.; Rae, Ian D.
Australian Journal of Chemistry, 1987 , vol. 40, # 8 p. 1477 - 1481
