2-(溴甲基)丙烯酸甲酯合成路线 （共 27 条）
反应条件
phosphorus tribromide in diethyl ether Inert atmosphere;
参考文献
Luehr, Susan; Holz, Jens; Zayas, Odalys; Seidelmann, Oliver; Domke, Lutz; Boerner, Armin
Tetrahedron Asymmetry, 2013 , vol. 24, # 7 p. 395 - 401
反应条件
N-bromosuccinmide; sodium chloride in diethyl ether; dichloromethane
参考文献
Barrera, Jaime Bermejo; Silva, Margarita Hernandez; De Mon, Melchor Alvarez; Ranieri, Juan Pablo Pivel
Patent: US2003/199575 A1, 2003 ;
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in tetrachloromethane T=0°C; 1 h;
参考文献
Charlton, J. L.; Sayeed, V. A.; Lypka, G. N.
Synthetic Communications, 1981 , vol. 11, # 11 p. 931 - 934
反应条件
N,N'-dibromo-N,N'-1,2-ethylene bis(2,5-dimethylbenzene sulfonamide); dibenzoyl peroxide in tetrachloromethane T=20°C; 1 h;
参考文献
Khazaei, Ardeshir; Vaghei, Ramin Ghorbani; Karkhanei, Ebrahim
Synthetic Communications, 2002 , vol. 32, # 14 p. 2107 - 2113
反应条件
sulfuric acid; hydrogen bromide
参考文献
Drewes, Siegfried E.; Loizou, Georgia; Roos, Gregory H. P.
Synthetic Communications, 1987 , vol. 17, # 3 p. 291 - 298
反应条件
1: diethyl 2,2-bis(hydroxymethyl)malonate With hydrogen bromide 2: methanol With sulfuric acid in toluene
参考文献
Yu, Haibo; Yang, Huibin; Cui, Dongliang; Lv, Liang; Li, Bin
Journal of Agricultural and Food Chemistry, 2011 , vol. 59, # 21 p. 11718 - 11726
反应条件
sodium hydride 1) DMF, 0 deg C, then rt, 0.5 h, 2) rt, 24 h; Yield given. Multistep reaction;
参考文献
Yang, Cangming; Murray, William V.; Wilson, Lawrence J.
Tetrahedron Letters, 2003 , vol. 44, # 9 p. 1783 - 1786
反应条件
potassium carbonate in methanol; Petroleum ether
参考文献
SCHERING CORPORATION
Patent: WO2007/97937 A1, 2007 ;
Location in patent: Page/Page column 204 ;
WO 2007/097937 A1
反应条件
potassium carbonate in Petroleum ether
参考文献
SCHERING CORPORATION
Patent: WO2007/70398 A1, 2007 ;
Location in patent: Page/Page column 241 ;
WO 2007/070398 A1
反应条件
2: EtCHO / methanol View Scheme
参考文献
Duettmann,H.; Weyerstahl,P.
Chemische Berichte, 1979 , vol. 112, p. 3480 - 3485
