1-氯-1,1,2,2,3,3,3-七氟丙烷合成路线 (共 23 条)
参考文献
Kinetic Chem.Inc.
Patent: US2490764 , 1945 ;
反应条件
chlorine
Irradiation.mit UV-Licht;
参考文献
Haszeldine
Journal of the Chemical Society, 1953 , p. 3761,3766
反应条件
chlorine
T=50 - 100°C;
参考文献
Hauptschein et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 1347,1350
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Haszeldine; Steele
Journal of the Chemical Society, 1953 , p. 1592,1597
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Haszeldine
Journal of the Chemical Society, 1952 , p. 4259,4266
Journal of the Chemical Society, 1953 , p. 3761,3767
反应条件
d-limonene; aluminum chlorofluoride
T=15.4 - 40.2°C; P=1085.86 Torr; 0.72 h; Product distribution / selectivity;
参考文献
E.I.DU PONT DE NEMOURS AND COMPANY
Patent: WO2008/54780 A2, 2008 ;
Location in patent: Page/Page column 17 ;
参考文献
Husted; Kohlhase
Journal of the American Chemical Society, 1954 , vol. 76, p. 5141,5143
反应条件
aluminum chlorofluoride in various solvent(s)
T=50°C; Addition; 16 h; Title compound not separated from byproducts;
参考文献
Petrov, Viacheslav A.; Krespan, Carl G.
Journal of Fluorine Chemistry, 2000 , vol. 102, # 1-2 p. 199 - 204
反应条件
aluminum chlorofluoride
T=37 - 41°C; P=3759.59 Torr; 4 h; Product distribution / selectivity;
参考文献
E.I.DU PONT DE NEMOURS AND COMPANY
Patent: WO2008/54780 A2, 2008 ;
Location in patent: Page/Page column 16-17 ;
反应条件
hydrogen; fluorided platinum on aluminum oxide
T=250°C; Product distribution / selectivity;
参考文献
E.I.DU PONT DE NEMOURS AND COMPANY
Patent: WO2008/54780 A2, 2008 ;
Location in patent: Page/Page column 21-22 ;
反应条件
chlorine
T=500 - 530°C;
参考文献
Minnesota Mining and Mfg.Co.
Patent: US2658928 , 1947 ;
参考文献
Kinetic Chem.Inc.
Patent: US2490764 , 1945 ;