2,2,3,3,3-五氟-1-丙醇合成路线 （共 52 条）
反应条件
hydrogen; Rh/C in water T=20 - 90°C; P=7500.75 Torr; 18 h;
参考文献
SOLVAY (Societe Anonyme)
Patent: EP1820789 A1, 2007 ;
Location in patent: Page/Page column 3 ;
反应条件
lithium aluminium tetrahydride in anhydrous butyl ether
参考文献
Gmelin Handbook: F: PerFHalOrg.7, 1, page 1 - 84
反应条件
water; zinc; fluorad FC-143 T=27 - 29°C; 1 h; Product distribution / selectivity;
参考文献
Daikin Industries, Ltd.
Patent: EP2078709 A1, 2009 ;
Location in patent: Page/Page column 5-6 ;
反应条件
RuHCl(CO)(bis-(2-diphenylphosphinoethyl)amine); hydrogen; sodium methylate in methanol T=40°C; P=7600.51 Torr; 22 h; AutoclaveInert atmosphere;
参考文献
Otsuka, Takashi; Ishii, Akihiro; Dub, Pavel A.; Ikariya, Takao
Journal of the American Chemical Society, 2013 , vol. 135, # 26 p. 9600 - 9603
反应条件
RuHCl(CO)(bis-(2-diphenylphosphinoethyl)amine); hydrogen; sodium methylate in methanol T=40°C; P=3800.26 Torr; 22 h; AutoclaveInert atmosphere;
参考文献
Central Glass Company, Limited; ISHII, Akihiro; OOTSUKA, Takashi; IMAMURA, Mari; NISHIMIYA, Takayuki; KIMURA, Kazuto
Patent: EP2740719 A1, 2014 ;
Location in patent: Paragraph 0058 ;
参考文献
McBee et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 1378,1389
反应条件
sulfuric acid; hydrogen fluoride T=50°C;
参考文献
Weinmayr,V.
Journal of Organic Chemistry, 1963 , vol. 28, p. 492 - 494
反应条件
vinylidene difluoride; hydrogen fluoride
参考文献
Weinmayr,V.
Journal of Organic Chemistry, 1963 , vol. 28, p. 492 - 494
参考文献
McBee et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 1387,1390
参考文献
McBee et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 86
