反应条件
in diethyl ether
mixt. stirred over 0.2 h; heated under reflux overnight; cooled, treated with CHCl3/water; aq. layer extd. (CHCl3); org. ext. dried; washed (ethoxyethane); recrystd. (propanone/ethanol);
参考文献
Probitts, E. Jane; Saunders, David R.; Stone, Michael H.; Mawby, Roger J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1986 , p. 1167 - 1174