2-(4-氯-丁基)-异吲哚-1,3-二酮合成路线 (共 7 条)
参考文献
Keil
Chemische Berichte, 1930 , vol. 63, p. 1614
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 238, p. 2169
反应条件
in N,N-dimethyl-formamide
T=20°C; 20 h; Inert atmosphere;
参考文献
Kadi, Nadia; Arbache, Simon; Song, Lijiang; Oves-Costales, Daniel; Challis, Gregory L.
Journal of the American Chemical Society, 2008 , vol. 130, # 32 p. 10458 - 10459
反应条件
sodium hydrogencarbonate; triethylamine in isopropyl alcohol
参考文献
Mitsubishi Gas Chemical Co., Inc.
Patent: US5244487 A1, 1993 ;
反应条件
methanol; 1-chloroethyl chlorocarbonate
1) 1,2-dichloroethane, a) 0 deg C, b) RT, c) reflux, 30 min, 2) reflux, 1.5h; Yield given. Multistep reaction;
参考文献
Olofson, R. A.; Abbott, Duain E.
Journal of Organic Chemistry, 1984 , vol. 49, # 15 p. 2795 - 2799
参考文献
Keil
Chemische Berichte, 1930 , vol. 63, p. 1614
Full Text Show Details
Celanese Corp. Am.
Patent: US2571251 , 1946 ;
反应条件
acetone; sodium iodide
参考文献
Arnstein et al.
Journal of the Chemical Society, 1952 , p. 1329,1331
Org. Synth. Isotopes, 1958 , p. 274