2,4-二甲基-1-碘苯合成路线 (共 38 条)
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine in tetrahydrofuran
T=20°C; Inert atmosphere;
参考文献
Xu, Yanli; Zhao, Jinwu; Chen, Huoji; Wu, Wanqing; Jiang, Huanfeng
Chemical Communications, 2014 , vol. 50, # 19 p. 2488 - 2490
反应条件
copper(l) iodide; tetrabutylammomium bromide; potassium hydroxide
T=110°C; 6 h;
参考文献
Ali, Md. Ashif; Saha, Prasenjit; Punniyamurthy, Tharmalingam
Synthesis, 2010 , # 6 p. 908 - 910
反应条件
tetrachloromethane; sulfur dioxide; iodine; acetic acid
T=170 - 235°C; Reagens 4: rauchende Salpetersaeure;
参考文献
Hammerich
Chemische Berichte, 1890 , vol. 23, p. 1635
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Toehl; Bauch
Chemische Berichte, 1893 , vol. 26, p. 1106
参考文献
Bauch
Chemische Berichte, 1890 , vol. 23, p. 3117
反应条件
nickel in N,N-dimethyl-formamide
T=140°C; 78 h;
参考文献
Chao, C. S.; Cheng, C. H.; Chang, C. T.
Journal of Organic Chemistry, 1983 , vol. 48, # 25 p. 4904 - 4907
参考文献
Mascarelli; Longo
Gazzetta Chimica Italiana, 1941 , vol. 71, p. 389,392
反应条件
sulfur dioxide; nitric acid; acetic anhydride
参考文献
Varma; Raman
Journal of the Indian Chemical Society, 1935 , vol. 12, p. 540
反应条件
tetrabutyl-ammonium chloride; palladium diacetate; sodium hydrogencarbonate
T=80°C; 30 h;
参考文献
Gangjee, Aleem; Qiu, Yibin; Kisliuk, Roy L.
Journal of Heterocyclic Chemistry, 2004 , vol. 41, # 6 p. 941 - 946