1,1,1,2,3-五氯-2-氟丙烷合成路线 (共 6 条)
反应条件
1: With hydrogen fluoride T=130°C; 1 h; 2: With SbF5 T=120°C; 23 h;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2008/30438 A2, 2008 ;
Location in patent: Page/Page column 30 ;
反应条件
chlorine in tetrachloromethane
T=5°C; 4.5 h; UV-irradiation;
参考文献
ASAHI GLASS COMPANY, LIMITED
Patent: US2011/237846 A1, 2011 ;
Location in patent: Page/Page column 5 ;
反应条件
tetrachloromethane
beim Chlorieren im Sonnenlicht;
参考文献
Henne; Haeckl
Journal of the American Chemical Society, 1941 , vol. 63, p. 2692
反应条件
chlorine
Irradiation;
参考文献
Fainberg,A.H.; Miller,W.T.
Journal of Organic Chemistry, 1965 , vol. 30, p. 864 - 876
反应条件
beim Chlorieren im Sonnenlicht;
参考文献
Henne; Haeckl
Journal of the American Chemical Society, 1941 , vol. 63, p. 2692
反应条件
1: With hydrogen fluoride
T=130°C; 1 h;
2: With SbF5
T=120°C; 23 h;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2008/30438 A2, 2008 ;
Location in patent: Page/Page column 30 ;