DL-1-(2-呋喃基)乙醇合成路线 （共 62 条）
反应条件
[Ru(CO)2Cl(C5Bn5)]; potassium tert-butylate; sodium carbonate in tetrahydrofuran; toluene T=23°C; 9 h; Inert atmospheredynamic kinetic resolutionEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
European Journal of Organic Chemistry, , # 8 p. 1452 - 1457
反应条件
Candida antarctica lipase B; (η5-C5Ph5)Ru(CO)2Cl; potassium tert-butylate; sodium carbonate in tetrahydrofuran; toluene T=20°C; 6 h;
参考文献
Journal of the American Chemical Society, , vol. 127, # 24 p. 8817 - 8825
反应条件
Candida antarctica lipase B in toluene T=23°C; 1.5 h; Resolution of racemate; optical yield given as percent ee;
参考文献
European Journal of Organic Chemistry, , # 9 p. 1317 - 1320
反应条件
in hexane 24 h; lipozyme-IM;
参考文献
Tetrahedron Asymmetry, , vol. 7, # 3 p. 907 - 910
反应条件
Pseudomonas cepacia lipase; 4 A molecular sieve; peracetylated-β-cyclodextrin in toluene T=40°C; 8 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 14, # 17 p. 2547 - 2555
反应条件
Pseudomonas fluorescence Amano AKG lipase in cyclohexane T=36°C; 2 h;
参考文献
Synthetic Communications, , vol. 37, # 13 p. 2163 - 2170
反应条件
Lipase PS Amano from Burkholderia cepacia in di-isopropyl ether T=25°C; 24 h; Resolution of racemateIonic liquidsolid phase reactionEnzymatic reaction; optical yield given as percent ee;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 67, # 1-2 p. 129 - 134
反应条件
modified β-cyclodextrin colyophilized Amano AKG lipase in cyclohexane T=36°C; 2 h;
参考文献
Synthetic Communications, , vol. 37, # 13 p. 2163 - 2170
反应条件
2: pyridine View Scheme
参考文献
Journal of Organic Chemistry, , vol. 53, # 7 p. 1586 - 1587
反应条件
Pseudomonas cepacia lipase; peracetylated-β-cyclodextrin in toluene T=40°C; 8 h; Product distribution; Further Variations:Solventstimes;
参考文献
Tetrahedron Asymmetry, , vol. 12, # 19 p. 2761 - 2766
