DL-1-(2-呋喃基)乙醇合成路线 (共 62 条)
反应条件
1: methyl iodide With magnesium in diethyl ether Reflux; 2: furfural in diethyl ether T=-45°C; 0.5 h; 3: With sodium hydrogensulfite in diethyl ether; water Cooling with ice;
参考文献
Tetrahedron, , vol. 67, # 15 p. 2779 - 2787
反应条件
magnesium in tetrahydrofuran
反应条件
sodium tetrahydroborate in methanol T=0°C;
参考文献
Tetrahedron Asymmetry, , vol. 7, # 3 p. 907 - 910
参考文献
Journal of the Chemical Society, Chemical Communications, , # 10 p. 735 - 736
反应条件
in tetrahydrofuran T=0°C;
参考文献
Synlett, , # 10 art. no. S02605ST, p. 1547 - 1550
反应条件
potassium fluoride; tetraethylene glycol T=20°C; 4 h; chemoselective reaction;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 23 p. 8119 - 8121
反应条件
1: furfural; methyl-magnesium chloride in tetrahydrofuran T=0°C; 1.5 h; 2: 1,3,5-benzenetricarbonyl trichloride in tetrahydrofuran 1.33333 h;
参考文献
US2004/242724 A1, ;
Page 9 ;
反应条件
bis(acetylacetonate)nickel(II); triphenylphosphine in tetrahydrofuran; hexane T=0°C; 0.5 h;
参考文献
Chemistry Letters, , # 10 p. 1033 - 1034
反应条件
[Ru(CO)2Cl(C5Bn5)]; potassium tert-butylate; sodium carbonate in toluene
参考文献
European Journal of Organic Chemistry, , # 9 p. 1317 - 1320