3-甲基-2-丁烯酸-2-苯乙酯合成路线 （共 5 条）
反应条件
caesium carbonate; 1-tert-butylperoxy-1,2-benziodoxol-3(1H)-one in cyclohexane
T=25°C; 46 h;
参考文献
Ochiai, Masahito; Ito, Takao; Takahashi, Hideo; Nakanishi, Akinobu; Toyonari, Mika; Sueda, Takuya; Goto, Satoru; Shiro, Motoo
Journal of the American Chemical Society, 1996 , vol. 118, # 33 p. 7716 - 7730
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane
T=0 - 20°C; 3.83333 h;
参考文献
Tokuyasu, Takahiro; Kunikawa, Shigeki; McCullough, Kevin J.; Masuyama, Araki; Nojima, Masatomo
Journal of Organic Chemistry, 2005 , vol. 70, # 1 p. 251 - 260
反应条件
1: tetrabutylammonium iodide
2: 76 percent / 1-(tert-butylperoxy)-1,2-benziodoxol-3(1H)-one, Cs2CO3 / cyclohexane / 46 h / 25 °C
View Scheme
参考文献
Ochiai, Masahito; Ito, Takao; Takahashi, Hideo; Nakanishi, Akinobu; Toyonari, Mika; Sueda, Takuya; Goto, Satoru; Shiro, Motoo
Journal of the American Chemical Society, 1996 , vol. 118, # 33 p. 7716 - 7730
反应条件
1: tetrabutylammonium iodide
2: 76 percent / 1-(tert-butylperoxy)-1,2-benziodoxol-3(1H)-one, Cs2CO3 / cyclohexane / 46 h / 25 °C
View Scheme
参考文献
Ochiai, Masahito; Ito, Takao; Takahashi, Hideo; Nakanishi, Akinobu; Toyonari, Mika; Sueda, Takuya; Goto, Satoru; Shiro, Motoo
Journal of the American Chemical Society, 1996 , vol. 118, # 33 p. 7716 - 7730
反应条件
(i) aq. NH3, AgNO3, (ii) /BRN= 507487/, benzene; Multistep reaction;
参考文献
Cheng,Y.S.; von Rudloff,E.
Phytochemistry (Elsevier), 1970 , vol. 9, p. 2517 - 2527
