4-乙酰基-3-羟基乙酸苯酯合成路线 (共 18 条)
反应条件
trichlorophosphate in N-methyl-acetamide
参考文献
Takeda Chemical Industries, Ltd.
Patent: US3984441 A1, 1976 ;
反应条件
trichlorophosphate T=50°C; Vilsmeier-Haack Formylation; 13 h;
参考文献
Chand, Karam; Prasad, Suchita; Tiwari, Rakesh K.; Shirazi, Amir N.; Kumar, Sumit; Parang, Keykavous; Sharma, Sunil K.
Bioorganic Chemistry, 2014 , vol. 53, p. 75 - 82
参考文献
Lahoti, R. J.; Wagle, D. R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 11 p. 1007 - 1008
反应条件
nickel in ethanol; water 5 h; Heating / reflux;
参考文献
UNILEVER PLC; UNILEVER NV; HINDUSTAN LEVER LIMITED; HARICHIAN, Bijan
Patent: WO2004/52827 A1, 2004 ;
Location in patent: Page 9 ;
反应条件
1: K2CO3; acetone; KI 2: aqueous methanol.NaOH View Scheme
参考文献
Jurd; Rolle
Journal of the American Chemical Society, 1958 , vol. 80, p. 5527,5528
参考文献
Journal of the Chemical Society, , p. 1681,1683
参考文献
Baker; Jukes; Subrahmanyam
Journal of the Chemical Society, 1934 , p. 1681,1683
反应条件
1: bromine
2: aqueous methanol.NaOH
View Scheme
参考文献
Kaneniwa
Yakugaku Zasshi, 1955 , vol. 75, p. 785
Yakugaku Zasshi, 1955 , vol. 75, p. 791,794
Chem.Abstr., 1956 , p. 4842